(S)-6-(3-(2-(tert-butoxycarbonyl(methyl)amino)propyl)phenoxy)hexanoic acid

Base Information

Chemical Name:(S)-6-(3-(2-(tert-butoxycarbonyl(methyl)amino)propyl)phenoxy)hexanoic acid
CAS No.:1313762-88-7
Molecular Formula:C₂₁H₃₃NO₅
Molecular Weight:379.497
Hs Code.:

Synonyms:(S)-6-(3-(2-(tert-butoxycarbonyl(methyl)amino)propyl)phenoxy)hexanoic acid

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Chemical Property of (S)-6-(3-(2-(tert-butoxycarbonyl(methyl)amino)propyl)phenoxy)hexanoic acid

Chemical Property:

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Technology Process of (S)-6-(3-(2-(tert-butoxycarbonyl(methyl)amino)propyl)phenoxy)hexanoic acid

There total 7 articles about (S)-6-(3-(2-(tert-butoxycarbonyl(methyl)amino)propyl)phenoxy)hexanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1313762-83-2
(S)-1-(3-methoxyphenyl)-N-methyl-N-((S)-1-phenylethyl)-propan-2-amine

: 1313762-88-7
(S)-6-(3-(2-(tert-butoxycarbonyl(methyl)amino)propyl)phenoxy)hexanoic acid

Guidance literature:: Multi-step reaction with 5 steps

1: 5%-palladium/activated carbon; ammonium formate / methanol / 4 h / 50 °C

2: boron tribromide / dichloromethane / -78 - 25 °C

3: triethylamine / methanol / 0.5 h / Reflux

4: sodium hydride / hexanes; N,N-dimethyl-formamide / 16 h

5: lithium hydroxide monohydrate; water / tetrahydrofuran; methanol / 8 h / Reflux

With lithium hydroxide monohydrate; 5%-palladium/activated carbon; water; ammonium formate; boron tribromide; sodium hydride; triethylamine; In tetrahydrofuran; methanol; hexanes; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm2004943

Reference yield:

: 1313762-86-5
(S)-tert-butyl [1-(3-hydroxyphenyl)propan-2-yl](methyl)carbamate

: 1313762-88-7
(S)-6-(3-(2-(tert-butoxycarbonyl(methyl)amino)propyl)phenoxy)hexanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / hexanes; N,N-dimethyl-formamide / 16 h

2: lithium hydroxide monohydrate; water / tetrahydrofuran; methanol / 8 h / Reflux

With lithium hydroxide monohydrate; water; sodium hydride; In tetrahydrofuran; methanol; hexanes; N,N-dimethyl-formamide;
DOI:10.1021/jm2004943

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1313762-88-7
(S)-6-(3-(2-(tert-butoxycarbonyl(methyl)amino)propyl)phenoxy)hexanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / methanol / 0.5 h / Reflux

2: sodium hydride / hexanes; N,N-dimethyl-formamide / 16 h

3: lithium hydroxide monohydrate; water / tetrahydrofuran; methanol / 8 h / Reflux

With lithium hydroxide monohydrate; water; sodium hydride; triethylamine; In tetrahydrofuran; methanol; hexanes; N,N-dimethyl-formamide;
DOI:10.1021/jm2004943