C₃₉H₄₆N₂O₈

Base Information

Chemical Name:C₃₉H₄₆N₂O₈
CAS No.:1002095-50-2
Molecular Formula:C₃₉H₄₆N₂O₈
Molecular Weight:670.803
Hs Code.:

C<sub>39</sub>H<sub>46</sub>N<sub>2</sub>O<sub>8</sub>

Synonyms:C₃₉H₄₆N₂O₈

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Chemical Property of C₃₉H₄₆N₂O₈

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Technology Process of C₃₉H₄₆N₂O₈

There total 9 articles about C₃₉H₄₆N₂O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1002095-33-1
C₄₂H₅₀N₂O₈

: 1002095-50-2
C₃₉H₄₆N₂O₈

Guidance literature:: toluene-4-sulfonic acid; In methanol; at 20 ℃; for 40h;
DOI:10.1021/ja077853c

Reference yield:

: 1002095-31-9
C₃₄H₄₄N₂O₇

: 1002095-50-2
C₃₉H₄₆N₂O₈

Guidance literature:: Multi-step reaction with 3 steps

1: ammonium chloride; zinc / ethanol; water / 90 °C

2: sodium hydrogencarbonate / 1,4-dioxane; water / 4 h / 0 °C

3: toluene-4-sulfonic acid / methanol / 48 h / 20 °C

With sodium hydrogencarbonate; ammonium chloride; toluene-4-sulfonic acid; zinc; In 1,4-dioxane; methanol; ethanol; water;
DOI:10.1021/jo200553g

Reference yield:

: 100-39-0
benzyl bromide

: 1002095-50-2
C₃₉H₄₆N₂O₈

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1.25 h / 0 °C / Inert atmosphere

1.2: 3 h / Inert atmosphere

2.1: iodine; magnesium; ethylene dibromide / tetrahydrofuran / Reflux

2.2: 5 h / -50 °C

3.1: ammonium chloride; zinc / ethanol; water / 90 °C

4.1: sodium hydrogencarbonate / 1,4-dioxane; water / 4 h / 0 °C

5.1: toluene-4-sulfonic acid / methanol / 48 h / 20 °C

With iodine; sodium hydride; sodium hydrogencarbonate; ammonium chloride; toluene-4-sulfonic acid; magnesium; ethylene dibromide; zinc; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; water; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/jo200553g