2,3-di-O-acetyl-4,6-O-(p-methoxybenzylidene)-α-D-glucopyranosyl bromide

Base Information

Chemical Name:2,3-di-O-acetyl-4,6-O-(p-methoxybenzylidene)-α-D-glucopyranosyl bromide
CAS No.:316790-25-7
Molecular Formula:C₁₈H₂₁BrO₈
Molecular Weight:445.264
Hs Code.:

Synonyms:2,3-di-O-acetyl-4,6-O-(p-methoxybenzylidene)-α-D-glucopyranosyl bromide

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Chemical Property of 2,3-di-O-acetyl-4,6-O-(p-methoxybenzylidene)-α-D-glucopyranosyl bromide

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Technology Process of 2,3-di-O-acetyl-4,6-O-(p-methoxybenzylidene)-α-D-glucopyranosyl bromide

There total 1 articles about 2,3-di-O-acetyl-4,6-O-(p-methoxybenzylidene)-α-D-glucopyranosyl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 2,3-di-O-acetyl-4,6-O-(p-methoxybenzylidene)-α,β-D-glucopyranose

: 316790-25-7
2,3-di-O-acetyl-4,6-O-(p-methoxybenzylidene)-α-D-glucopyranosyl bromide

Guidance literature:: With pyridine; triphenyl phosphite; bromine; In dichloromethane; at 20 ℃; for 1.5h;
DOI:10.1021/jo0012952

Reference yield: 95.0%

: 316790-25-7
2,3-di-O-acetyl-4,6-O-(p-methoxybenzylidene)-α-D-glucopyranosyl bromide

: (2R,4aR,6R,8R,8aS)-2-(4-methoxyphenyl)hexahydropyrano[3,2-d][1,3]dioxine-6,8-diyl-7-d diacetate

: C₁₈H₂₁⁽²⁾HO₈

Guidance literature:: With tetrahydrofuran-d8; tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate; at 20 ℃; for 20h; regioselective reaction; Sealed tube; Irradiation; Schlenk technique; Inert atmosphere;
DOI:10.1021/jacs.0c11209

Reference yield: 89.0%

: 316790-25-7
2,3-di-O-acetyl-4,6-O-(p-methoxybenzylidene)-α-D-glucopyranosyl bromide

: 316790-21-3
[(10S)-2-undecyn-10-yl]-3,4,6-tri-O-(p-methoxybenzyl)-β-D-glucopyranoside

: 316790-26-8
Acetic acid (2R,4aR,6S,7R,8S,8aR)-8-acetoxy-6-[(2R,3R,4S,5R,6R)-4,5-bis-(4-methoxy-benzyloxy)-6-(4-methoxy-benzyloxymethyl)-2-((S)-1-methyl-dec-8-ynyloxy)-tetrahydro-pyran-3-yloxy]-2-(4-methoxy-phenyl)-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl ester

Guidance literature:: With 2,6-di-tert-butyl-pyridine; 4 A molecular sieve; silver trifluoromethanesulfonate; In dichloromethane; at -5 ℃; for 3h;
DOI:10.1021/jo0012952