N-[(benzotriazol-1-yl)-p-tolylmethyl]-p-toluenesulfonamide

Base Information

• Chemical Name: N-[(benzotriazol-1-yl)-p-tolylmethyl]-p-toluenesulfonamide
• CAS No.: 188564-49-0
• Molecular Formula: C₂₁H₂₀N₄O₂S
• Molecular Weight: 392.481
• Mol file: 188564-49-0.mol

Synonyms:N-[(benzotriazol-1-yl)-p-tolylmethyl]-p-toluenesulfonamide

Chemical Property of N-[(benzotriazol-1-yl)-p-tolylmethyl]-p-toluenesulfonamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-[(benzotriazol-1-yl)-p-tolylmethyl]-p-toluenesulfonamide

There total 1 articles about N-[(benzotriazol-1-yl)-p-tolylmethyl]-p-toluenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

1,2,3-Benzotriazole (95-14-7,27556-51-0) + 4-methyl-benzaldehyde (104-87-0) + toluene-4-sulfonamide (70-55-3) → N-[(benzotriazol-1-yl)-p-tolylmethyl]-p-toluenesulfonamide (188564-49-0)

Guidance literature:

With toluene-4-sulfonic acid; In toluene; for 48h; Heating;

DOI:10.1080/00397919708004211

Reference yield: 96.0%

allyl bromide (106-95-6) + N-[(benzotriazol-1-yl)-p-tolylmethyl]-p-toluenesulfonamide (188564-49-0) → 4-methyl-N-(1-p-tolylbut-3-enyl)benzenesulfonamide (243671-17-2)

Guidance literature:

allyl bromide; With samarium; iodine; In tetrahydrofuran; at 20 ℃; for 1h;

N-[(benzotriazol-1-yl)-p-tolylmethyl]-p-toluenesulfonamide; In tetrahydrofuran; at 20 ℃; for 0.0833333h;

DOI:10.1081/SCC-120024744

Reference yield: 95.0%

potassium cyanide (151-50-8) + N-[(benzotriazol-1-yl)-p-tolylmethyl]-p-toluenesulfonamide (188564-49-0) → N-[cyano(p-tolyl)methyl]-4-methylbenzenesulfonamide

Guidance literature:

In water; for 24h;

DOI:10.1080/00397919708004211

upstream raw materials:

1,2,3-Benzotriazole

4-methyl-benzaldehyde

toluene-4-sulfonamide

Downstream raw materials:

4-methyl-N-(1-p-tolylbut-3-enyl)benzenesulfonamide

N-p-xylyl-p-toluenesulfonamide