2-[(3-bromo-5-chlorophenyl)oxy]-4-(bromomethyl)-1-chloro-3-fluorobenzene

Base Information

Chemical Name:2-[(3-bromo-5-chlorophenyl)oxy]-4-(bromomethyl)-1-chloro-3-fluorobenzene
CAS No.:1093262-86-2
Molecular Formula:C₁₃H₇Br₂Cl₂FO
Molecular Weight:428.91
Hs Code.:

Synonyms:2-[(3-bromo-5-chlorophenyl)oxy]-4-(bromomethyl)-1-chloro-3-fluorobenzene

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Chemical Property of 2-[(3-bromo-5-chlorophenyl)oxy]-4-(bromomethyl)-1-chloro-3-fluorobenzene

Chemical Property:

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Technology Process of 2-[(3-bromo-5-chlorophenyl)oxy]-4-(bromomethyl)-1-chloro-3-fluorobenzene

There total 6 articles about 2-[(3-bromo-5-chlorophenyl)oxy]-4-(bromomethyl)-1-chloro-3-fluorobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1093262-84-0
2-[(3-bromo-5-chlorophenyl)oxy]-1-chloro-3-fluoro-4-methylbenzene

: 1093262-86-2
2-[(3-bromo-5-chlorophenyl)oxy]-4-(bromomethyl)-1-chloro-3-fluorobenzene

: 1190959-69-3
2-[(3-bromo-5-chlorophenyl)oxy]-4-(dibromomethyl)-1-chloro-3-fluorobenzene

Guidance literature:: With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); In tetrachloromethane; at 90 ℃; for 6h; Inert atmosphere;

Reference yield:

: 1093262-77-1
bis(1,1-dimethylethyl) {3-[(3-bromo-5-chlorophenyl)oxy]-2-fluoro-4-nitrophenyl}propanedioate

: 1093262-86-2
2-[(3-bromo-5-chlorophenyl)oxy]-4-(bromomethyl)-1-chloro-3-fluorobenzene

: 1190959-69-3
2-[(3-bromo-5-chlorophenyl)oxy]-4-(dibromomethyl)-1-chloro-3-fluorobenzene

Guidance literature:: Multi-step reaction with 5 steps

1: trifluoroacetic acid / dichloromethane / 3 h / 40 °C

2: copper(I) oxide / acetonitrile / 3 h / Reflux

3: sodium dithionite / tetrahydrofuran; water / 16 h / 40 °C

4: tert.-butylnitrite; copper dichloride / acetonitrile / 0.5 h / 50 °C / Inert atmosphere

5: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / tetrachloromethane / 6 h / 90 °C / Inert atmosphere

With copper(I) oxide; N-Bromosuccinimide; tert.-butylnitrite; sodium dithionite; 2,2'-azobis(isobutyronitrile); trifluoroacetic acid; copper dichloride; In tetrahydrofuran; tetrachloromethane; dichloromethane; water; acetonitrile;

Reference yield:

: 1093262-79-3
{3-[(3-bromo-5-chlorophenyl)oxy]-2-fluoro-4-nitrophenyl}acetic acid

: 1093262-86-2
2-[(3-bromo-5-chlorophenyl)oxy]-4-(bromomethyl)-1-chloro-3-fluorobenzene

: 1190959-69-3
2-[(3-bromo-5-chlorophenyl)oxy]-4-(dibromomethyl)-1-chloro-3-fluorobenzene

Guidance literature:: Multi-step reaction with 4 steps

1: copper(I) oxide / acetonitrile / 3 h / Reflux

2: sodium dithionite / tetrahydrofuran; water / 16 h / 40 °C

3: tert.-butylnitrite; copper dichloride / acetonitrile / 0.5 h / 50 °C / Inert atmosphere

4: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / tetrachloromethane / 6 h / 90 °C / Inert atmosphere

With copper(I) oxide; N-Bromosuccinimide; tert.-butylnitrite; sodium dithionite; 2,2'-azobis(isobutyronitrile); copper dichloride; In tetrahydrofuran; tetrachloromethane; water; acetonitrile;