N-(1-naphthyl)-N,N'-diphenyl-N'-(4-((4-vinylphenyl)methoxymethyl)phenyl)benzidine

Base Information

Chemical Name:N-(1-naphthyl)-N,N'-diphenyl-N'-(4-((4-vinylphenyl)methoxymethyl)phenyl)benzidine
CAS No.:849146-84-5
Molecular Formula:C₅₀H₄₀N₂O
Molecular Weight:684.88
Hs Code.:

Synonyms:N-(1-naphthyl)-N,N'-diphenyl-N'-(4-((4-vinylphenyl)methoxymethyl)phenyl)benzidine

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Chemical Property of N-(1-naphthyl)-N,N'-diphenyl-N'-(4-((4-vinylphenyl)methoxymethyl)phenyl)benzidine

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Technology Process of N-(1-naphthyl)-N,N'-diphenyl-N'-(4-((4-vinylphenyl)methoxymethyl)phenyl)benzidine

There total 8 articles about N-(1-naphthyl)-N,N'-diphenyl-N'-(4-((4-vinylphenyl)methoxymethyl)phenyl)benzidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 849146-80-1
N-(1-naphthyl)-N,N'-diphenyl-N'-(4-(hydroxymethyl)phenyl)benzidine

: 1592-20-7,29296-32-0
4-Vinylbenzyl chloride

: 849146-84-5
N-(1-naphthyl)-N,N'-diphenyl-N'-(4-((4-vinylphenyl)methoxymethyl)phenyl)benzidine

Guidance literature:: N-(1-naphthyl)-N,N'-diphenyl-N'-(4-(hydroxymethyl)phenyl)benzidine; With potassium; In toluene; at 100 ℃; for 3h;

4-Vinylbenzyl chloride; In toluene; at 90 ℃; for 20h;
DOI:10.1021/ma048365h

Reference yield:

: 352359-42-3
N-(4’-bromo-[1,1‘-biphenyl]-4-yl)-N-phenylnaphthalen-1-amine

: 849146-84-5
N-(1-naphthyl)-N,N'-diphenyl-N'-(4-((4-vinylphenyl)methoxymethyl)phenyl)benzidine

Guidance literature:: Multi-step reaction with 4 steps

1.1: 90 percent / t-BuONa; DPPF / Pd₂(dba)3 / toluene / 6 h / 100 °C

2.1: t-BuONa; p(tBu)3 / Pd₂(dba)3 / toluene / 5 h / 100 °C

3.1: 10.12 g / Bu₄NF / tetrahydrofuran; H₂O / 2 h / 20 °C

4.1: K / toluene / 3 h / 100 °C

4.2: 61 percent / toluene / 20 h / 90 °C

With 1,1'-bis-(diphenylphosphino)ferrocene; tri-tert-butyl phosphine; tetrabutyl ammonium fluoride; potassium; sodium t-butanolate; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; In tetrahydrofuran; water; toluene;
DOI:10.1021/ma048365h

Reference yield:

: 873-75-6
4-bromobenzenemethanol

: 849146-84-5
N-(1-naphthyl)-N,N'-diphenyl-N'-(4-((4-vinylphenyl)methoxymethyl)phenyl)benzidine

Guidance literature:: Multi-step reaction with 4 steps

1.1: 96 percent / pyridine / CH₂Cl₂ / 5 h / 20 °C

2.1: t-BuONa; p(tBu)3 / Pd₂(dba)3 / toluene / 5 h / 100 °C

3.1: 10.12 g / Bu₄NF / tetrahydrofuran; H₂O / 2 h / 20 °C

4.1: K / toluene / 3 h / 100 °C

4.2: 61 percent / toluene / 20 h / 90 °C

With pyridine; tri-tert-butyl phosphine; tetrabutyl ammonium fluoride; potassium; sodium t-butanolate; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; In tetrahydrofuran; dichloromethane; water; toluene;
DOI:10.1021/ma048365h