4-(1-(N-(2,2-diethoxyethyl)amino)-2-(benzyloxy)ethyl)-1,2-dimethoxybenzene

Base Information

Chemical Name:4-(1-(N-(2,2-diethoxyethyl)amino)-2-(benzyloxy)ethyl)-1,2-dimethoxybenzene
CAS No.:147624-55-3
Molecular Formula:C₂₃H₃₃NO₅
Molecular Weight:403.519
Hs Code.:

Synonyms:4-(1-(N-(2,2-diethoxyethyl)amino)-2-(benzyloxy)ethyl)-1,2-dimethoxybenzene

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Chemical Property of 4-(1-(N-(2,2-diethoxyethyl)amino)-2-(benzyloxy)ethyl)-1,2-dimethoxybenzene

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Technology Process of 4-(1-(N-(2,2-diethoxyethyl)amino)-2-(benzyloxy)ethyl)-1,2-dimethoxybenzene

There total 8 articles about 4-(1-(N-(2,2-diethoxyethyl)amino)-2-(benzyloxy)ethyl)-1,2-dimethoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 645-36-3
2,2-diethoxy-ethanamine

: 147624-54-2
(benzyloxy)methyl-3,4-dimethoxyphenyl ketone

: 147624-55-3
4-(1-(N-(2,2-diethoxyethyl)amino)-2-(benzyloxy)ethyl)-1,2-dimethoxybenzene

Guidance literature:: With sodium cyanoborohydride; magnesium sulfate; In methanol; acetic acid; Heating;
DOI:10.1080/00397919308009802

Reference yield: 81.0%

: 1448706-86-2
N-(2,2-diethoxyethyl)-2-(3,4-dimethoxyphenyl)glycinol

: 100-39-0
benzyl bromide

: 147624-55-3
4-(1-(N-(2,2-diethoxyethyl)amino)-2-(benzyloxy)ethyl)-1,2-dimethoxybenzene

Guidance literature:: N-(2,2-diethoxyethyl)-2-(3,4-dimethoxyphenyl)glycinol; With potassium hydride; In tetrahydrofuran; paraffin oil;

benzyl bromide; In tetrahydrofuran; paraffin oil; at 0 - 20 ℃; for 5h;
DOI:10.3987/COM-12-S(N)59

Reference yield:

: 140687-75-8,102104-61-0
2-(3,4-dimethoxyphenyl)oxirane

: 147624-55-3
4-(1-(N-(2,2-diethoxyethyl)amino)-2-(benzyloxy)ethyl)-1,2-dimethoxybenzene

Guidance literature:: Multi-step reaction with 3 steps

1: 61 percent / phenylmethanol / 100 °C

2: 90 percent / NaOAc, PCC/Al₂O₃ / CH₂Cl₂ / Heating

3: 95 percent / NaCNBH₃, MgSO₄ / acetic acid; methanol / Heating

With aluminum oxide; sodium acetate; sodium cyanoborohydride; magnesium sulfate; pyridinium chlorochromate; In methanol; dichloromethane; acetic acid; benzyl alcohol;
DOI:10.1080/00397919308009802