C₂₆H₃₄O₄Si

Base Information

Chemical Name:C₂₆H₃₄O₄Si
CAS No.:1209497-06-2
Molecular Formula:C₂₆H₃₄O₄Si
Molecular Weight:438.639
Hs Code.:

C<sub>26</sub>H<sub>34</sub>O<sub>4</sub>Si

Synonyms:C₂₆H₃₄O₄Si

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Chemical Property of C₂₆H₃₄O₄Si

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Technology Process of C₂₆H₃₄O₄Si

There total 10 articles about C₂₆H₃₄O₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1040918-08-8
(3aR,6aR)-6-(tert-butyldiphenylsiloxymethyl)-2,2,3a-trimethyl-3a,6a-dihydrocyclopenta[1,3]dioxol-4-one

: 1209497-06-2
C₂₆H₃₄O₄Si

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In ethyl acetate; for 20h; under 760.051 Torr;
DOI:10.1002/ejoc.201100062

Reference yield:

: 1209497-00-6
(1R,4'S,5'S)-1-(5'-tert-butyldiphenylsiloxymethyl)-(2',2'-dimethyl-5'-vinyl[1',3']dioxol-4'-yl)prop-2-en-1-ol

: 1209497-06-2
C₂₆H₃₄O₄Si

Guidance literature:: Multi-step reaction with 9 steps

1.1: Umicore M₂ / dichloromethane / 70 h / 20 °C / Inert atmosphere; Darkness

2.1: dipyridinium dichromate / dichloromethane / 72 h / 20 °C / Molecular sieve

3.1: tetrahydrofuran / 0.5 h / -78 °C

3.2: 2 h / 20 °C

4.1: bromine / dichloromethane / 2 h / 20 °C

4.2: 0.33 h / 20 °C

4.3: 16 h / -78 - -30 °C

5.1: potassium carbonate / methanol / 12 h / 20 °C

6.1: N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid / 1,2-dichloro-ethane / -30 - 20 °C / Reflux

7.1: sodium methylate / methanol / 0.25 h / -30 - 0 °C

8.1: toluene-4-sulfonic acid; 2,2-dimethoxy-propane / 13 h / 20 °C

9.1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 20 h / 760.05 Torr

With dipyridinium dichromate; palladium 10% on activated carbon; hydrogen; bromine; sodium methylate; potassium carbonate; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; 2,2-dimethoxy-propane; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate; 1,2-dichloro-ethane;
DOI:10.1002/ejoc.201100062

Reference yield:

: 1209497-01-7
(3aR,6aS)-6a-(tert-butyldiphenylsiloxymethyl)-2,2-dimethyl-3a,6a-dihydrocyclopenta[1,3]dioxol-4-one

: 1209497-06-2
C₂₆H₃₄O₄Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: tetrahydrofuran / 0.5 h / -78 °C

1.2: 2 h / 20 °C

2.1: bromine / dichloromethane / 2 h / 20 °C

2.2: 0.33 h / 20 °C

2.3: 16 h / -78 - -30 °C

3.1: potassium carbonate / methanol / 12 h / 20 °C

4.1: N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid / 1,2-dichloro-ethane / -30 - 20 °C / Reflux

5.1: sodium methylate / methanol / 0.25 h / -30 - 0 °C

6.1: toluene-4-sulfonic acid; 2,2-dimethoxy-propane / 13 h / 20 °C

7.1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 20 h / 760.05 Torr

With palladium 10% on activated carbon; hydrogen; bromine; sodium methylate; potassium carbonate; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; 2,2-dimethoxy-propane; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate; 1,2-dichloro-ethane;
DOI:10.1002/ejoc.201100062