cis-3-amino-4-(hydroxymethyl)-trans-2-(4-methoxyphenyl)tetrahydrothiophene

Base Information

Chemical Name:cis-3-amino-4-(hydroxymethyl)-trans-2-(4-methoxyphenyl)tetrahydrothiophene
CAS No.:128869-59-0
Molecular Formula:C₁₂H₁₇NO₂S
Molecular Weight:239.338
Hs Code.:

Synonyms:cis-3-amino-4-(hydroxymethyl)-trans-2-(4-methoxyphenyl)tetrahydrothiophene

Suppliers and Price of cis-3-amino-4-(hydroxymethyl)-trans-2-(4-methoxyphenyl)tetrahydrothiophene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of cis-3-amino-4-(hydroxymethyl)-trans-2-(4-methoxyphenyl)tetrahydrothiophene

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of cis-3-amino-4-(hydroxymethyl)-trans-2-(4-methoxyphenyl)tetrahydrothiophene

There total 4 articles about cis-3-amino-4-(hydroxymethyl)-trans-2-(4-methoxyphenyl)tetrahydrothiophene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 127865-46-7
6-(4-methoxyphenyl)-3,3a,4,6-tetrahydrothiopheno<3,4-c>isoxazole

: 128869-59-0
cis-3-amino-4-(hydroxymethyl)-trans-2-(4-methoxyphenyl)tetrahydrothiophene

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; for 6h; Heating;
DOI:10.1021/jo00307a023

Reference yield:

: 3179-10-0
1-methoxy-4-(2-nitro-vinyl)-benzene

: 128869-59-0
cis-3-amino-4-(hydroxymethyl)-trans-2-(4-methoxyphenyl)tetrahydrothiophene

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / piperidine / diethyl ether

2: triethylamine, phenyl isocyanate / benzene / Ambient temperature

3: 85 percent / LiAlH₄ / diethyl ether / 6 h / Heating

With piperidine; lithium aluminium tetrahydride; phenyl isocyanate; triethylamine; In diethyl ether; benzene;
DOI:10.1021/jo00307a023

Reference yield:

: 127865-40-1
2-(allylthio)-2-(4-methoxyphenyl)-1-nitroethane

: 128869-59-0
cis-3-amino-4-(hydroxymethyl)-trans-2-(4-methoxyphenyl)tetrahydrothiophene

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine, phenyl isocyanate / benzene / Ambient temperature

2: 85 percent / LiAlH₄ / diethyl ether / 6 h / Heating

With lithium aluminium tetrahydride; phenyl isocyanate; triethylamine; In diethyl ether; benzene;
DOI:10.1021/jo00307a023