N-[6-(2,6-dichlorophenyl)-2-methylpyrido[2,3-d]-pyrimidin-7-yl]-N'-N-dimethylguanidine

Base Information

Chemical Name:N-[6-(2,6-dichlorophenyl)-2-methylpyrido[2,3-d]-pyrimidin-7-yl]-N'-N-dimethylguanidine
CAS No.:77206-79-2
Molecular Formula:C₁₇H₁₆Cl₂N₆
Molecular Weight:375.26
Hs Code.:

Synonyms:N-[6-(2,6-dichlorophenyl)-2-methylpyrido[2,3-d]-pyrimidin-7-yl]-N'-N-dimethylguanidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[6-(2,6-dichlorophenyl)-2-methylpyrido[2,3-d]-pyrimidin-7-yl]-N'-N-dimethylguanidine

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Technology Process of N-[6-(2,6-dichlorophenyl)-2-methylpyrido[2,3-d]-pyrimidin-7-yl]-N'-N-dimethylguanidine

There total 3 articles about N-[6-(2,6-dichlorophenyl)-2-methylpyrido[2,3-d]-pyrimidin-7-yl]-N'-N-dimethylguanidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 29.0%

: 77206-77-0
N-<6-(2,6-dichlorophenyl)-2-methylpyrido<2,3-d>pyrimidin-7-yl>-N'-methylthiourea

: 74-89-5
methylamine

: 77206-79-2
N-[6-(2,6-Dichloro-phenyl)-2-methyl-pyrido[2,3-d]pyrimidin-7-yl]-N',N''-dimethyl-guanidine

Guidance literature:: With mercury(II) oxide; In ethanol; for 0.333333h; Heating;
DOI:10.1021/jm00357a015

Reference yield:

: 21908-53-2,12653-71-3
mercury(II) oxide

: 77206-77-0
N-<6-(2,6-dichlorophenyl)-2-methylpyrido<2,3-d>pyrimidin-7-yl>-N'-methylthiourea

: N-[6-(2,6-dichlorophenyl)-2-methylyrido[2,3-d]pyrimidin-7-yl]-N',N-dimethylguanidine

: 77206-79-2
N-[6-(2,6-dichlorophenyl)-2-methylpyrido[2,3-d]-pyrimidin-7-yl]-N'-N-dimethylguanidine

Guidance literature:: With methylamine; In ethanol;

Reference yield:

: 76574-80-6
6-(2,6-dichlorophenyl)-2-methylpyrido<2,3-d>pyrimidin-7-amine

: 77206-79-2
N-[6-(2,6-Dichloro-phenyl)-2-methyl-pyrido[2,3-d]pyrimidin-7-yl]-N',N''-dimethyl-guanidine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.5 g / toluene / 30 h / Heating

2: 29 percent / HgO / ethanol / 0.33 h / Heating

With mercury(II) oxide; In ethanol; toluene;
DOI:10.1021/jm00357a015