bis(benzoyl-η6-benzene)chromium

Base Information

Chemical Name:bis(benzoyl-η6-benzene)chromium
CAS No.:82556-00-1
Molecular Formula:C₂₆H₂₀CrO₂
Molecular Weight:416.44
Hs Code.:

Synonyms:bis(benzoyl-η6-benzene)chromium

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Chemical Property of bis(benzoyl-η6-benzene)chromium

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Technology Process of bis(benzoyl-η6-benzene)chromium

There total 3 articles about bis(benzoyl-η6-benzene)chromium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

: 233665-13-9
(Me3Sn-η6-C6H5)2Cr

: 98-88-4
benzoyl chloride

: 82556-00-1
bis(benzoyl-η6-benzene)chromium

Guidance literature:: With n-BuLi; In tetrahydrofuran; hexane; N2 atm.; molar ratio n-BuLi:13 =2:1, cooling (-78°C, 135 min), heating (room temp.);

Reference yield: 5.0%

: 1271-54-1
bis(benzene)chromium⁽⁰⁾

: 611-74-5
N,N-dimethylbenzamide

: 52445-45-1
(η-6-benzene)(benzoyl-η-6-benzene)chromium

: 82556-00-1
bis(benzoyl-η6-benzene)chromium

Guidance literature:: With n-butyllithium; air; water; In hexane; methyl cyclohexane; (N2); (C6H6)2Cr was lithiated; addn. of N,N-dimethylbenzamide with stirring; stirring for 24 h at 25°C; hydrolysis (2 h ); oxidn. with air in H2O/CH3OH soln.; extn. with toluene, redn. of the water phase with Na2S2O4; repeated extn. with toluene, extract washed with water, dried; sepn. by chromy; recrystn. from petroleum ether (40-60°C) / benzene; elem. anal.;