N-(2-bromoallyl)-4-methyl-N-(3-((4-methylphenyl)sulfonamido)propyl)benzenesulfonamide

Base Information

Chemical Name:N-(2-bromoallyl)-4-methyl-N-(3-((4-methylphenyl)sulfonamido)propyl)benzenesulfonamide
CAS No.:1443366-04-8
Molecular Formula:C₂₀H₂₅BrN₂O₄S₂
Molecular Weight:501.465
Hs Code.:

Synonyms:N-(2-bromoallyl)-4-methyl-N-(3-((4-methylphenyl)sulfonamido)propyl)benzenesulfonamide

Suppliers and Price of N-(2-bromoallyl)-4-methyl-N-(3-((4-methylphenyl)sulfonamido)propyl)benzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(2-bromoallyl)-4-methyl-N-(3-((4-methylphenyl)sulfonamido)propyl)benzenesulfonamide

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Technology Process of N-(2-bromoallyl)-4-methyl-N-(3-((4-methylphenyl)sulfonamido)propyl)benzenesulfonamide

There total 4 articles about N-(2-bromoallyl)-4-methyl-N-(3-((4-methylphenyl)sulfonamido)propyl)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1443366-02-6
C₂₅H₃₃BrN₂O₆S₂

: 1443366-04-8
N-(2-bromoallyl)-4-methyl-N-(3-((4-methylphenyl)sulfonamido)propyl)benzenesulfonamide

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 0 ℃;
DOI:10.1002/adsc.201200703

Reference yield:

: 176107-53-2
N,N'-bis(p-toluenesulfonamido)-N-(tert-butoxycarbonyl)-1,3-propanediamine

: 1443366-04-8
N-(2-bromoallyl)-4-methyl-N-(3-((4-methylphenyl)sulfonamido)propyl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; tetra-(n-butyl)ammonium iodide / water; toluene

2: trifluoroacetic acid / dichloromethane / 0 °C

With tetra(n-butyl)ammonium hydrogensulfate; tetra-(n-butyl)ammonium iodide; trifluoroacetic acid; sodium hydroxide; In dichloromethane; water; toluene;
DOI:10.1002/adsc.201200703

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 1443366-04-8
N-(2-bromoallyl)-4-methyl-N-(3-((4-methylphenyl)sulfonamido)propyl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / dichloromethane

2: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran

3: sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; tetra-(n-butyl)ammonium iodide / water; toluene

4: trifluoroacetic acid / dichloromethane / 0 °C

With di-isopropyl azodicarboxylate; tetra(n-butyl)ammonium hydrogensulfate; tetra-(n-butyl)ammonium iodide; triethylamine; triphenylphosphine; trifluoroacetic acid; sodium hydroxide; In tetrahydrofuran; dichloromethane; water; toluene;
DOI:10.1002/adsc.201200703