N-(2-bromoallyl)-4-methyl-N-(3-(4-methyl-N-(oct-1-yn-1-yl)phenylsulfonamido)propyl)benzenesulfonamide

Base Information

Chemical Name:N-(2-bromoallyl)-4-methyl-N-(3-(4-methyl-N-(oct-1-yn-1-yl)phenylsulfonamido)propyl)benzenesulfonamide
CAS No.:1443365-63-6
Molecular Formula:C₂₈H₃₇BrN₂O₄S₂
Molecular Weight:609.649
Hs Code.:

Synonyms:N-(2-bromoallyl)-4-methyl-N-(3-(4-methyl-N-(oct-1-yn-1-yl)phenylsulfonamido)propyl)benzenesulfonamide

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Chemical Property of N-(2-bromoallyl)-4-methyl-N-(3-(4-methyl-N-(oct-1-yn-1-yl)phenylsulfonamido)propyl)benzenesulfonamide

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Technology Process of N-(2-bromoallyl)-4-methyl-N-(3-(4-methyl-N-(oct-1-yn-1-yl)phenylsulfonamido)propyl)benzenesulfonamide

There total 6 articles about N-(2-bromoallyl)-4-methyl-N-(3-(4-methyl-N-(oct-1-yn-1-yl)phenylsulfonamido)propyl)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 38761-67-0
1-bromo-1-octyne

: 1443366-04-8
N-(2-bromoallyl)-4-methyl-N-(3-((4-methylphenyl)sulfonamido)propyl)benzenesulfonamide

: 1443365-63-6
N-(2-bromoallyl)-4-methyl-N-(3-(4-methyl-N-(oct-1-yn-1-yl)phenylsulfonamido)propyl)benzenesulfonamide

Guidance literature:: With potassium phosphate; 1,10-Phenanthroline; copper(ll) sulfate pentahydrate; In toluene; at 85 ℃; for 48h;
DOI:10.1002/adsc.201200703

Reference yield:

: 176107-53-2
N,N'-bis(p-toluenesulfonamido)-N-(tert-butoxycarbonyl)-1,3-propanediamine

: 1443365-63-6
N-(2-bromoallyl)-4-methyl-N-(3-(4-methyl-N-(oct-1-yn-1-yl)phenylsulfonamido)propyl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; tetra-(n-butyl)ammonium iodide / water; toluene

2: trifluoroacetic acid / dichloromethane / 0 °C

3: 1,10-Phenanthroline; potassium phosphate; copper(ll) sulfate pentahydrate / toluene / 48 h / 85 °C

With potassium phosphate; 1,10-Phenanthroline; copper(ll) sulfate pentahydrate; tetra(n-butyl)ammonium hydrogensulfate; tetra-(n-butyl)ammonium iodide; trifluoroacetic acid; sodium hydroxide; In dichloromethane; water; toluene;
DOI:10.1002/adsc.201200703

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 1443365-63-6
N-(2-bromoallyl)-4-methyl-N-(3-(4-methyl-N-(oct-1-yn-1-yl)phenylsulfonamido)propyl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 5 steps

1: triethylamine / dichloromethane

2: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran

3: sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; tetra-(n-butyl)ammonium iodide / water; toluene

4: trifluoroacetic acid / dichloromethane / 0 °C

5: 1,10-Phenanthroline; potassium phosphate; copper(ll) sulfate pentahydrate / toluene / 48 h / 85 °C

With potassium phosphate; 1,10-Phenanthroline; copper(ll) sulfate pentahydrate; di-isopropyl azodicarboxylate; tetra(n-butyl)ammonium hydrogensulfate; tetra-(n-butyl)ammonium iodide; triethylamine; triphenylphosphine; trifluoroacetic acid; sodium hydroxide; In tetrahydrofuran; dichloromethane; water; toluene;
DOI:10.1002/adsc.201200703