(S)-3-Methyl-2-[1-phenyl-eth-(E)-ylideneamino]-butyric acid tert-butyl ester

Base Information

Chemical Name:(S)-3-Methyl-2-[1-phenyl-eth-(E)-ylideneamino]-butyric acid tert-butyl ester
CAS No.:59903-75-2
Molecular Formula:C₁₇H₂₅NO₂
Molecular Weight:275.391
Hs Code.:

Synonyms:(S)-3-Methyl-2-[1-phenyl-eth-(E)-ylideneamino]-butyric acid tert-butyl ester

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Chemical Property of (S)-3-Methyl-2-[1-phenyl-eth-(E)-ylideneamino]-butyric acid tert-butyl ester

Chemical Property:

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Technology Process of (S)-3-Methyl-2-[1-phenyl-eth-(E)-ylideneamino]-butyric acid tert-butyl ester

There total 1 articles about (S)-3-Methyl-2-[1-phenyl-eth-(E)-ylideneamino]-butyric acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13211-31-9
tert-butyl L-valinate

: 98-86-2
acetophenone

: 59903-75-2
(S)-3-Methyl-2-[1-phenyl-eth-(E)-ylideneamino]-butyric acid tert-butyl ester

Guidance literature:: In benzene; for 72h; Heating;
DOI:10.1248/cpb.31.887

Reference yield:

: 59903-75-2
(S)-3-Methyl-2-[1-phenyl-eth-(E)-ylideneamino]-butyric acid tert-butyl ester

: 3886-69-9
(R)-1-phenyl-ethyl-amine

Guidance literature:: Multi-step reaction with 4 steps

1: H₂ / 5percent palladium on charcoal / ethanol / 16 h / Ambient temperature

2: tert-butyl hypochlorite / diethyl ether / 0.5 h / 0 °C

3: sodium ethoxide / ethanol / 1 h / 40 °C

4: 5percent sulfuric acid / H₂O / 2 h / Ambient temperature

With tert-butylhypochlorite; sulfuric acid; hydrogen; sodium ethanolate; palladium on activated charcoal; In diethyl ether; ethanol; water;
DOI:10.1248/cpb.31.887

Reference yield:

: 59903-75-2
(S)-3-Methyl-2-[1-phenyl-eth-(E)-ylideneamino]-butyric acid tert-butyl ester

: 2627-86-3
(S)-1-phenyl-ethylamine

Guidance literature:: Multi-step reaction with 4 steps

1: H₂ / 5percent palladium on charcoal / ethanol / 16 h / Ambient temperature

2: tert-butyl hypochlorite / diethyl ether / 0.5 h / 0 °C

3: sodium ethoxide / ethanol / 1 h / 40 °C

4: 5percent sulfuric acid / H₂O / 2 h / Ambient temperature

With tert-butylhypochlorite; sulfuric acid; hydrogen; sodium ethanolate; palladium on activated charcoal; In diethyl ether; ethanol; water;
DOI:10.1248/cpb.31.887