1-(3,4-Dimethoxyphenyl)-3-(methoxycarbonyl)-1,2,3,4-tetrahydro-β-carboline

Base Information

Chemical Name:1-(3,4-Dimethoxyphenyl)-3-(methoxycarbonyl)-1,2,3,4-tetrahydro-β-carboline
CAS No.:82789-36-4
Molecular Formula:C₂₁H₂₂N₂O₄
Molecular Weight:366.417
Hs Code.:

Synonyms:1-(3,4-Dimethoxyphenyl)-3-(methoxycarbonyl)-1,2,3,4-tetrahydro-β-carboline

Suppliers and Price of 1-(3,4-Dimethoxyphenyl)-3-(methoxycarbonyl)-1,2,3,4-tetrahydro-β-carboline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 1-(3,4-Dimethoxyphenyl)-3-(methoxycarbonyl)-1,2,3,4-tetrahydro-β-carboline

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of 1-(3,4-Dimethoxyphenyl)-3-(methoxycarbonyl)-1,2,3,4-tetrahydro-β-carboline

There total 5 articles about 1-(3,4-Dimethoxyphenyl)-3-(methoxycarbonyl)-1,2,3,4-tetrahydro-β-carboline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: L-Tryptophan Methyl Ester

: 120-14-9
3,4-dimethoxy-benzaldehyde

: 82789-36-4
1-(3,4-Dimethoxyphenyl)-3-(methoxycarbonyl)-1,2,3,4-tetrahydro-β-carboline

Guidance literature:: In toluene; for 20h; Heating;
DOI:10.1002/jhet.5570240449

Reference yield:

: 54-12-6,27732-43-0,80206-30-0,27813-82-7
Trp

: 82789-36-4
1-(3,4-Dimethoxyphenyl)-3-(methoxycarbonyl)-1,2,3,4-tetrahydro-β-carboline

Guidance literature:: Multi-step reaction with 2 steps

1.1: Reflux

2.1: thionyl chloride / 1 h / 0 °C

2.2: 65 °C

With thionyl chloride; 1.1: |Pictet-Spengler Synthesis;
DOI:10.1016/j.ejmech.2019.02.054

Reference yield:

: 67-56-1
methanol

: 82789-27-3
1-(3,4-dimethoxyphenyl)-2,3,4,9-tetrahydro-1H-beta-carboline-3-carboxylic acid

: 82789-36-4
1-(3,4-Dimethoxyphenyl)-3-(methoxycarbonyl)-1,2,3,4-tetrahydro-β-carboline

Guidance literature:: methanol; 1-(3,4-dimethoxyphenyl)-2,3,4,9-tetrahydro-1H-beta-carboline-3-carboxylic acid; With thionyl chloride; at 0 ℃; for 1h;

at 65 ℃;
DOI:10.1016/j.ejmech.2019.02.054