2'-deoxy-N⁶,5'-O-bis{[2-(4-nitrophenyl)ethoxy]carbonyl}adenosine 3'-[2-(4-nitrophenyl)ethyl diisopropylphosphoramidite]

Base Information

• Chemical Name: 2'-deoxy-N⁶,5'-O-bis{[2-(4-nitrophenyl)ethoxy]carbonyl}adenosine 3'-[2-(4-nitrophenyl)ethyl diisopropylphosphoramidite]
• CAS No.: 153120-91-3
• Molecular Formula: C₄₂H₄₈N₉O₁₄P
• Molecular Weight: 933.869

Synonyms:2'-deoxy-N⁶,5'-O-bis{[2-(4-nitrophenyl)ethoxy]carbonyl}adenosine 3'-[2-(4-nitrophenyl)ethyl diisopropylphosphoramidite]

Chemical Property of 2'-deoxy-N⁶,5'-O-bis{[2-(4-nitrophenyl)ethoxy]carbonyl}adenosine 3'-[2-(4-nitrophenyl)ethyl diisopropylphosphoramidite]

Chemical Property:

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Technology Process of 2'-deoxy-N⁶,5'-O-bis{[2-(4-nitrophenyl)ethoxy]carbonyl}adenosine 3'-[2-(4-nitrophenyl)ethyl diisopropylphosphoramidite]

There total 1 articles about 2'-deoxy-N⁶,5'-O-bis{[2-(4-nitrophenyl)ethoxy]carbonyl}adenosine 3'-[2-(4-nitrophenyl)ethyl diisopropylphosphoramidite] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

2'-deoxy-N6,5'-O-bis<2-(4-nitrophenyl)ethoxycarbonyl>adenosine + 2-(4-nitrophenyl)ethyl diisopropylphosphoramidochloridite (153120-90-2) → 2'-deoxy-N6,5'-O-bis{[2-(4-nitrophenyl)ethoxy]carbonyl}adenosine 3'-[2-(4-nitrophenyl)ethyl diisopropylphosphoramidite] (153120-91-3)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 1.5h;

DOI:10.1002/hlca.200390186

Reference yield: 93.0%

2'-deoxy-N6,5'-O-bis{[2-(4-nitrophenyl)ethoxy]carbonyl}adenosine 3'-[2-(4-nitrophenyl)ethyl diisopropylphosphoramidite] (153120-91-3) + 2'-deoxy-N6-[(9H-fluoren-9-ylmethoxy)carbonyl]adenylyl-{3'-{OP-[2-(4-nitrophenyl)ethyl]}-5'}-2'-deoxy-N6,3'-O-bis{[2-(4-nitrophenyl)ethoxy]carbonyl}adenosine (153120-95-7) → C97H89N21O35P2 (153120-96-8)

Guidance literature:

2'-deoxy-N⁶,5'-O-bis{[2-(4-nitrophenyl)ethoxy]carbonyl}adenosine 3'-[2-(4-nitrophenyl)ethyl diisopropylphosphoramidite]; 2'-deoxy-N⁶-[(9H-fluoren-9-ylmethoxy)carbonyl]adenylyl-{3'-{O^P-[2-(4-nitrophenyl)ethyl]}-5'}-2'-deoxy-N⁶,3'-O-bis{[2-(4-nitrophenyl)ethoxy]carbonyl}adenosine; With 1H-tetrazole; In dichloromethane; acetonitrile; at 20 ℃; for 2h;

With pyridine; iodine; In various solvents; for 0.25h;

DOI:10.1002/hlca.200390186

Reference yield: 84.0%

2'-deoxy-N6,5'-O-bis{[2-(4-nitrophenyl)ethoxy]carbonyl}adenosine 3'-[2-(4-nitrophenyl)ethyl diisopropylphosphoramidite] (153120-91-3) + C91H78N17O30P → C127H111N25O45P2

Guidance literature:

2'-deoxy-N⁶,5'-O-bis{[2-(4-nitrophenyl)ethoxy]carbonyl}adenosine 3'-[2-(4-nitrophenyl)ethyl diisopropylphosphoramidite]; C₉₁H₇₈N₁₇O₃₀P; With 1H-tetrazole; In dichloromethane; acetonitrile; at 20 ℃; for 1.5h;

With iodine; In various solvents; for 0.25h;

DOI:10.1002/hlca.200390186

upstream raw materials:

2-(4-nitrophenyl)ethyl diisopropylphosphoramidochloridite

Downstream raw materials:

C₉₇H₈₉N₂₁O₃₅P₂

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