C₃₅H₅₅N₉O₆S₂

Base Information

Chemical Name:C₃₅H₅₅N₉O₆S₂
CAS No.:1259040-35-1
Molecular Formula:C₃₅H₅₅N₉O₆S₂
Molecular Weight:762.01
Hs Code.:

C<sub>35</sub>H<sub>55</sub>N<sub>9</sub>O<sub>6</sub>S<sub>2</sub>

Synonyms:C₃₅H₅₅N₉O₆S₂

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Chemical Property of C₃₅H₅₅N₉O₆S₂

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Technology Process of C₃₅H₅₅N₉O₆S₂

There total 16 articles about C₃₅H₅₅N₉O₆S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1259040-34-0
C₃₀H₄₅N₉O₆S₂

: 96-22-0
pentan-3-one

: 1259040-35-1
C₃₅H₅₅N₉O₆S₂

Guidance literature:: C₃₀H₄₅N₉O₆S₂; pentan-3-one; With titanium(IV) tetraethanolate; In tetrahydrofuran; at 50 ℃; for 1h; Inert atmosphere;

With sodium tris(acetoxy)borohydride; In tetrahydrofuran; at 20 ℃; for 1h;

With sodium carbonate; In tetrahydrofuran; water;

Reference yield:

: 1228603-43-7
4-(2-oxoethyl)-piperidine-1,4-dicarboxylic acid 1-tert-butyl ester 4-ethyl ester

: 1259040-35-1
C₃₅H₅₅N₉O₆S₂

Guidance literature:: Multi-step reaction with 12 steps

1.1: acetic acid; sodium tris(acetoxy)borohydride / N,N-dimethyl-formamide / 21 h / 20 - 40 °C / Inert atmosphere

2.1: diisobutylaluminium hydride / tetrahydrofuran / 2 h / -40 °C / Inert atmosphere

2.2: 0.5 h / -40 - 20 °C

3.1: lithium diisopropyl amide; N,N,N,N,N,N-hexamethylphosphoric triamide / n-heptane; tetrahydrofuran; ethylbenzene / 0.08 h / -78 °C / Inert atmosphere

3.2: 1.5 h

4.1: water; sodium tetrahydroborate / ethanol / 5 h / 20 °C

5.1: hydrogen / 10 wt% Pd(OH)2 on carbon / ethanol / 3 h / 60 °C

6.1: sodium carbonate / tetrahydrofuran / 3 h

7.1: triethanolamine; pyridine-SO₃ complex; dimethyl sulfoxide / dichloromethane / 24 h / 0 - 20 °C / Inert atmosphere

8.1: 2-methyl-but-2-ene; sodium hypochlorite; sodium dihydrogenphosphate / water; tert-butyl alcohol / 2.25 h / 20 °C

8.2: 0.02 h

9.1: hydrogen / 10 wt% Pd(OH)2 on carbon / ethanol / 0.5 h / 20 °C

10.1: water; α-picoline-borane / methanol / 4 h

11.1: water; sulfuric acid / methanol / 18 h / 0 - 20 °C

12.1: titanium(IV) tetraethanolate / tetrahydrofuran / 1 h / 50 °C / Inert atmosphere

12.2: 1 h / 20 °C

With N,N,N,N,N,N-hexamethylphosphoric triamide; titanium(IV) tetraethanolate; sodium hypochlorite; sodium tetrahydroborate; sodium dihydrogenphosphate; 2-methyl-but-2-ene; pyridine-SO₃ complex; triethanolamine; sulfuric acid; α-picoline-borane; water; hydrogen; sodium tris(acetoxy)borohydride; diisobutylaluminium hydride; sodium carbonate; acetic acid; dimethyl sulfoxide; lithium diisopropyl amide; 10 wt% Pd(OH)2 on carbon; In tetrahydrofuran; methanol; ethanol; n-heptane; dichloromethane; ethylbenzene; water; N,N-dimethyl-formamide; tert-butyl alcohol;

Reference yield:

: 146603-99-8
1-(1,1-dimethylethyl) 4-ethyl 4-(2-propenyl)-1,4-piperidinedicarboxylate

: 1259040-35-1
C₃₅H₅₅N₉O₆S₂

Guidance literature:: Multi-step reaction with 13 steps

1.1: ozone / methanol / 1 h / -78 °C

1.2: 15 h / 20 °C

2.1: acetic acid; sodium tris(acetoxy)borohydride / N,N-dimethyl-formamide / 21 h / 20 - 40 °C / Inert atmosphere

3.1: diisobutylaluminium hydride / tetrahydrofuran / 2 h / -40 °C / Inert atmosphere

3.2: 0.5 h / -40 - 20 °C

4.1: lithium diisopropyl amide; N,N,N,N,N,N-hexamethylphosphoric triamide / n-heptane; tetrahydrofuran; ethylbenzene / 0.08 h / -78 °C / Inert atmosphere

4.2: 1.5 h

5.1: water; sodium tetrahydroborate / ethanol / 5 h / 20 °C

6.1: hydrogen / 10 wt% Pd(OH)2 on carbon / ethanol / 3 h / 60 °C

7.1: sodium carbonate / tetrahydrofuran / 3 h

8.1: triethanolamine; pyridine-SO₃ complex; dimethyl sulfoxide / dichloromethane / 24 h / 0 - 20 °C / Inert atmosphere

9.1: 2-methyl-but-2-ene; sodium hypochlorite; sodium dihydrogenphosphate / water; tert-butyl alcohol / 2.25 h / 20 °C

9.2: 0.02 h

10.1: hydrogen / 10 wt% Pd(OH)2 on carbon / ethanol / 0.5 h / 20 °C

11.1: water; α-picoline-borane / methanol / 4 h

12.1: water; sulfuric acid / methanol / 18 h / 0 - 20 °C

13.1: titanium(IV) tetraethanolate / tetrahydrofuran / 1 h / 50 °C / Inert atmosphere

13.2: 1 h / 20 °C

With N,N,N,N,N,N-hexamethylphosphoric triamide; titanium(IV) tetraethanolate; sodium hypochlorite; sodium tetrahydroborate; sodium dihydrogenphosphate; 2-methyl-but-2-ene; pyridine-SO₃ complex; triethanolamine; sulfuric acid; α-picoline-borane; water; hydrogen; sodium tris(acetoxy)borohydride; diisobutylaluminium hydride; sodium carbonate; ozone; acetic acid; dimethyl sulfoxide; lithium diisopropyl amide; 10 wt% Pd(OH)2 on carbon; In tetrahydrofuran; methanol; ethanol; n-heptane; dichloromethane; ethylbenzene; water; N,N-dimethyl-formamide; tert-butyl alcohol;