2,2'-[{[4-(diethoxymethyl)benzyl]imino}bis(methylene)]bis(N,N-dimethyl-1H-imidazole-1-sulfonamide)

Base Information

Chemical Name:2,2'-[{[4-(diethoxymethyl)benzyl]imino}bis(methylene)]bis(N,N-dimethyl-1H-imidazole-1-sulfonamide)
CAS No.:937074-59-4
Molecular Formula:C₂₄H₃₇N₇O₆S₂
Molecular Weight:583.733
Hs Code.:

Synonyms:2,2'-[{[4-(diethoxymethyl)benzyl]imino}bis(methylene)]bis(N,N-dimethyl-1H-imidazole-1-sulfonamide)

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Chemical Property of 2,2'-[{[4-(diethoxymethyl)benzyl]imino}bis(methylene)]bis(N,N-dimethyl-1H-imidazole-1-sulfonamide)

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Technology Process of 2,2'-[{[4-(diethoxymethyl)benzyl]imino}bis(methylene)]bis(N,N-dimethyl-1H-imidazole-1-sulfonamide)

There total 1 articles about 2,2'-[{[4-(diethoxymethyl)benzyl]imino}bis(methylene)]bis(N,N-dimethyl-1H-imidazole-1-sulfonamide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 937074-59-4
2,2'-[{[4-(diethoxymethyl)benzyl]imino}bis(methylene)]bis(N,N-dimethyl-1H-imidazole-1-sulfonamide)

Guidance literature:

Reference yield:

: 937074-59-4
2,2'-[{[4-(diethoxymethyl)benzyl]imino}bis(methylene)]bis(N,N-dimethyl-1H-imidazole-1-sulfonamide)

: 1259039-31-0
2,2'-[[(4-formylbenzyl)imino]bis(methylene)]bis(N,N-dimethyl-1H-imidazole-1-sulfonamide)

Guidance literature:: 2,2'-[{[4-(diethoxymethyl)benzyl]imino}bis(methylene)]bis(N,N-dimethyl-1H-imidazole-1-sulfonamide); With hydrogenchloride; water; In ethyl acetate; at 20 ℃; for 0.05h;

With sodium carbonate; In water; ethyl acetate;

Reference yield:

: 937074-59-4
2,2'-[{[4-(diethoxymethyl)benzyl]imino}bis(methylene)]bis(N,N-dimethyl-1H-imidazole-1-sulfonamide)

: 1259039-34-3
8-tert-butyl 3-ethyl (3R)-2-(4-{[bis({1-[(dimethylamino)sulfonyl]-1H-imidazol-2-yl}methyl)amino]methyl}benzyl)-2,8-diazaspiro[4.5]decane-3,8-dicarboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogenchloride; water / ethyl acetate / 0.05 h / 20 °C

2: sodium tetrahydroborate; methanol / tetrahydrofuran / 2 h / Inert atmosphere

3: N-ethyl-N,N-diisopropylamine; methanesulfonyl chloride; lithium chloride / tetrahydrofuran / 1 h / 0 - 20 °C

4: N-ethyl-N,N-diisopropylamine / acetonitrile / 15 h / 50 °C / Inert atmosphere

With hydrogenchloride; methanol; sodium tetrahydroborate; water; methanesulfonyl chloride; N-ethyl-N,N-diisopropylamine; lithium chloride; In tetrahydrofuran; ethyl acetate; acetonitrile;