5-(1,3-benzodioxol-5-yl)-1-[(2,4-dichlorophenyl)sulfonyl]-1H-tetrazole

Base Information

Chemical Name:5-(1,3-benzodioxol-5-yl)-1-[(2,4-dichlorophenyl)sulfonyl]-1H-tetrazole
CAS No.:1358577-77-1
Molecular Formula:C₁₄H₈Cl₂N₄O₄S
Molecular Weight:399.214
Hs Code.:

Synonyms:5-(1,3-benzodioxol-5-yl)-1-[(2,4-dichlorophenyl)sulfonyl]-1H-tetrazole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-(1,3-benzodioxol-5-yl)-1-[(2,4-dichlorophenyl)sulfonyl]-1H-tetrazole

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Technology Process of 5-(1,3-benzodioxol-5-yl)-1-[(2,4-dichlorophenyl)sulfonyl]-1H-tetrazole

There total 4 articles about 5-(1,3-benzodioxol-5-yl)-1-[(2,4-dichlorophenyl)sulfonyl]-1H-tetrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 118923-32-3
5-[3',4'-(methylenedioxy)benzen-1'-yl]-1H-tetrazole

: 16271-33-3
2,4-Dichlorobenzenesulfonyl chloride

: 1358577-77-1
5-(1,3-benzodioxol-5-yl)-1-[(2,4-dichlorophenyl)sulfonyl]-1H-tetrazole

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1016/j.ejmech.2011.12.033

Reference yield:

: 2089-36-3,20747-41-5,20747-42-6
(E)-3,4-methylenedioxybenzaldehyde oxime

: 1358577-77-1
5-(1,3-benzodioxol-5-yl)-1-[(2,4-dichlorophenyl)sulfonyl]-1H-tetrazole

Guidance literature:: Multi-step reaction with 3 steps

1: acetic anhydride / Reflux

2: sodium azide; zinc dibromide / water; isopropyl alcohol / 24 h / Reflux

3: triethylamine / dichloromethane / 0 - 20 °C

With sodium azide; acetic anhydride; triethylamine; zinc dibromide; In dichloromethane; water; isopropyl alcohol;
DOI:10.1016/j.ejmech.2011.12.033

Reference yield:

: 120-57-0,30024-74-9
piperonal

: 1358577-77-1
5-(1,3-benzodioxol-5-yl)-1-[(2,4-dichlorophenyl)sulfonyl]-1H-tetrazole

Guidance literature:: Multi-step reaction with 4 steps

1: hydroxylamine hydrochloride; sodium hydrogencarbonate / water

2: acetic anhydride / Reflux

3: sodium azide; zinc dibromide / water; isopropyl alcohol / 24 h / Reflux

4: triethylamine / dichloromethane / 0 - 20 °C

With sodium azide; hydroxylamine hydrochloride; acetic anhydride; sodium hydrogencarbonate; triethylamine; zinc dibromide; In dichloromethane; water; isopropyl alcohol;
DOI:10.1016/j.ejmech.2011.12.033