thexyldimethylsilyl O-(6-O-benzyl-3,4-O-isopropylidene-β-D-galactopyranosyl)-(1->4)-[(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-(1->3)]-2-azido-6-O-benzyl-2-deoxy-β-D-glucopyranoside

Base Information

Chemical Name:thexyldimethylsilyl O-(6-O-benzyl-3,4-O-isopropylidene-β-D-galactopyranosyl)-(1->4)-[(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-(1->3)]-2-azido-6-O-benzyl-2-deoxy-β-D-glucopyranoside
CAS No.:228563-48-2
Molecular Formula:C₆₄H₈₃N₃O₁₄Si
Molecular Weight:1146.46
Hs Code.:

thexyldimethylsilyl O-(6-O-benzyl-3,4-O-isopropylidene-β-D-galactopyranosyl)-(1->4)-[(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-(1->3)]-2-azido-6-O-benzyl-2-deoxy-β-D-glucopyranoside

Synonyms:thexyldimethylsilyl O-(6-O-benzyl-3,4-O-isopropylidene-β-D-galactopyranosyl)-(1->4)-[(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-(1->3)]-2-azido-6-O-benzyl-2-deoxy-β-D-glucopyranoside

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Chemical Property of thexyldimethylsilyl O-(6-O-benzyl-3,4-O-isopropylidene-β-D-galactopyranosyl)-(1->4)-[(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-(1->3)]-2-azido-6-O-benzyl-2-deoxy-β-D-glucopyranoside

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Technology Process of thexyldimethylsilyl O-(6-O-benzyl-3,4-O-isopropylidene-β-D-galactopyranosyl)-(1->4)-[(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-(1->3)]-2-azido-6-O-benzyl-2-deoxy-β-D-glucopyranoside

There total 9 articles about thexyldimethylsilyl O-(6-O-benzyl-3,4-O-isopropylidene-β-D-galactopyranosyl)-(1->4)-[(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-(1->3)]-2-azido-6-O-benzyl-2-deoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 67-64-1
acetone

: 228563-47-1
thexyldimethylsilyl O-(6-O-benzyl-β-D-galactopyranosyl)-(1->4)-[(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-(1->3)]-2-azido-6-O-benzyl-2-deoxy-β-D-glucopyranoside

: 228563-48-2
thexyldimethylsilyl O-(6-O-benzyl-3,4-O-isopropylidene-β-D-galactopyranosyl)-(1->4)-[(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-(1->3)]-2-azido-6-O-benzyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: toluene-4-sulfonic acid; at 20 ℃; for 16h;

Reference yield:

: 1125-88-8
benzaldehyde dimethyl acetal

: 228563-48-2
thexyldimethylsilyl O-(6-O-benzyl-3,4-O-isopropylidene-β-D-galactopyranosyl)-(1->4)-[(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-(1->3)]-2-azido-6-O-benzyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 6 steps

1: 95 percent / p-TsOH / acetonitrile / 1 h / 20 °C

2: 85 percent / TMSOTf / diethyl ether

3: 80 percent / NaCNBH₃; HCl; molecular sieves / tetrahydrofuran; diethyl ether

4: 85 percent / TMSOTf / diethyl ether

5: 5.39 g / NaOMe / methanol

6: 96 percent / p-TsOH / 16 h / 20 °C

With hydrogenchloride; molecular sieve; sodium methylate; sodium cyanoborohydride; toluene-4-sulfonic acid; trimethylsilyl trifluoromethanesulfonate; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; diethyl ether; acetonitrile; 1: Substitution / 2: Substitution / 3: Reduction / 4: Substitution / 5: Deacetylation / 6: Substitution;

Reference yield:

: 157488-91-0
thexyldimethylsilyl 2-azido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside

: 228563-48-2
thexyldimethylsilyl O-(6-O-benzyl-3,4-O-isopropylidene-β-D-galactopyranosyl)-(1->4)-[(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-(1->3)]-2-azido-6-O-benzyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: 85 percent / TMSOTf / diethyl ether

2: 80 percent / NaCNBH₃; HCl; molecular sieves / tetrahydrofuran; diethyl ether

3: 85 percent / TMSOTf / diethyl ether

4: 5.39 g / NaOMe / methanol

5: 96 percent / p-TsOH / 16 h / 20 °C

With hydrogenchloride; molecular sieve; sodium methylate; sodium cyanoborohydride; trimethylsilyl trifluoromethanesulfonate; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; diethyl ether; 1: Substitution / 2: Reduction / 3: Substitution / 4: Deacetylation / 5: Substitution;