N-[3-(2,3-dihydro-1H-indol-1-yl)-3-phenylpropyl]-N,N-dimethylamine

Base Information

• Chemical Name: N-[3-(2,3-dihydro-1H-indol-1-yl)-3-phenylpropyl]-N,N-dimethylamine
• CAS No.: 915953-59-2
• Molecular Formula: C₁₉H₂₄N₂
• Molecular Weight: 280.413

Synonyms:N-[3-(2,3-dihydro-1H-indol-1-yl)-3-phenylpropyl]-N,N-dimethylamine

Chemical Property of N-[3-(2,3-dihydro-1H-indol-1-yl)-3-phenylpropyl]-N,N-dimethylamine

Chemical Property:

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Technology Process of N-[3-(2,3-dihydro-1H-indol-1-yl)-3-phenylpropyl]-N,N-dimethylamine

There total 2 articles about N-[3-(2,3-dihydro-1H-indol-1-yl)-3-phenylpropyl]-N,N-dimethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + 3-(2,3-dihydro-1H-indol-1-yl)-3-phenylpropylamine (1036637-53-2) → N-[3-(2,3-dihydro-1H-indol-1-yl)-3-phenylpropyl]-N,N-dimethylamine (915953-59-2)

Guidance literature:

formaldehyd; 3-(2,3-dihydro-1H-indol-1-yl)-3-phenylpropylamine; With sodium cyanoborohydride; In methanol; water; at 20 ℃; for 2h;

With acetic acid; In methanol; water; for 2h;

With sodium hydroxide; In methanol; water;

DOI:10.1021/ol8009286

Reference yield: 72.0%

1-indoline (496-15-1) + N,N-dimethyl-3-hydroxy-3-phenylpropylamine (5554-64-3) → N-[3-(2,3-dihydro-1H-indol-1-yl)-3-phenylpropyl]-N,N-dimethylamine (915953-59-2)

Guidance literature:

N,N-dimethyl-3-hydroxy-3-phenylpropylamine; With methanesulfonyl chloride; triethylamine; In acetonitrile; at 20 ℃; for 3h;

1-indoline; With potassium carbonate; at 20 ℃; for 14h; Further stages.;

DOI:10.1016/j.bmc.2006.08.039

Reference yield: 100.0%

N-[3-(2,3-dihydro-1H-indol-1-yl)-3-phenylpropyl]-N,N-dimethylamine (915953-59-2) → C19H22N2 (23130-89-4)

Guidance literature:

With manganese(IV) oxide; In dichloromethane; for 2h; Reflux; Inert atmosphere;

DOI:10.1021/ol8009286

upstream raw materials:

1-indoline

N,N-dimethyl-3-hydroxy-3-phenylpropylamine

formaldehyd

3-(2,3-dihydro-1H-indol-1-yl)-3-phenylpropylamine

Downstream raw materials:

C₁₉H₂₂N₂

1[3-(1H-indol-1-yl)-3-phenyl-propyl]-methyl-amine

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