11-p-clorophenyl-7,8,9,10-tetrahydroquinolino<3',2':4,5>thieno<3,2-d>pyrimidine-2,4(1H,3H)dithione

Base Information

• Chemical Name: 11-p-clorophenyl-7,8,9,10-tetrahydroquinolino<3',2':4,5>thieno<3,2-d>pyrimidine-2,4(1H,3H)dithione
• CAS No.: 135300-08-2
• Molecular Formula: C₁₉H₁₄ClN₃S₃
• Molecular Weight: 415.991

Synonyms:11-p-clorophenyl-7,8,9,10-tetrahydroquinolino<3',2':4,5>thieno<3,2-d>pyrimidine-2,4(1H,3H)dithione

Chemical Property of 11-p-clorophenyl-7,8,9,10-tetrahydroquinolino<3',2':4,5>thieno<3,2-d>pyrimidine-2,4(1H,3H)dithione

Chemical Property:

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Technology Process of 11-p-clorophenyl-7,8,9,10-tetrahydroquinolino<3',2':4,5>thieno<3,2-d>pyrimidine-2,4(1H,3H)dithione

There total 1 articles about 11-p-clorophenyl-7,8,9,10-tetrahydroquinolino<3',2':4,5>thieno<3,2-d>pyrimidine-2,4(1H,3H)dithione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

carbon disulfide (75-15-0,12122-00-8) + 3-amino-4-(p-chlorophenyl)-5,6,7,8-tetrahydrothieno<2,3-b>quinoline-2-carbonitrile (94833-68-8) → 11-p-clorophenyl-7,8,9,10-tetrahydroquinolino<3',2':4,5>thieno<3,2-d>pyrimidine-2,4(1H,3H)dithione (135300-08-2)

Guidance literature:

In pyridine; for 6h; Heating;

Reference yield: 86.0%

11-p-clorophenyl-7,8,9,10-tetrahydroquinolino<3',2':4,5>thieno<3,2-d>pyrimidine-2,4(1H,3H)dithione (135300-08-2) + chloroacetonitrile (107-14-2) → 2,4-di(cyanomethylthio)-11-p-chlorophenyl-7,8,9,10-tetrahydro-quinolino<3',2':4,5>thieno<3,2-d>pyrimidine (135300-17-3)

Guidance literature:

With sodium acetate; In ethanol; for 1h; Heating;

Reference yield: 85.0%

11-p-clorophenyl-7,8,9,10-tetrahydroquinolino<3',2':4,5>thieno<3,2-d>pyrimidine-2,4(1H,3H)dithione (135300-08-2) + chloroacetic acid ethyl ester (105-39-5) → 2,4-di(ethoxycarbonylmethylthio)-11-p-chlorophenyl-7,8,9,10-tetrahydro-quinolino<3',2':4,5>thieno<3,2-d>pyrimidine (135300-16-2)

Guidance literature:

With sodium acetate; In ethanol; for 1h; Heating;

upstream raw materials:

carbon disulfide

3-amino-4-(p-chlorophenyl)-5,6,7,8-tetrahydrothieno<2,3-b>quinoline-2-carbonitrile

Downstream raw materials:

2,4-di(cyanomethylthio)-11-p-chlorophenyl-7,8,9,10-tetrahydro-quinolino<3',2':4,5>thieno<3,2-d>pyrimidine

2,4-di(ethoxycarbonylmethylthio)-11-p-chlorophenyl-7,8,9,10-tetrahydro-quinolino<3',2':4,5>thieno<3,2-d>pyrimidine

2,4-di(N-phenylcarboxamidomethylthio)-11-p-chlorophenyl-7,8,9,10-tetrahydro-quinolino<3',2':4,5>thieno<3,2-d>pyrimidine

2,4-di(benzoylmethylthio)-11-p-chlorophenyl-7,8,9,10-tetrahydro-quinolino<3',2':4,5>thieno<3,2-d>pyrimidine

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