(2S-(2α(S*),3aα,4β,7β,7aα))-3-chloro-α-((octahydro-7,8,8-trimethyl-4,7-methano-benzofuran-2-yl)oxy)-4,5-di(phenylmethoxy)-benzeneethanamine

Base Information

Chemical Name:(2S-(2α(S*),3aα,4β,7β,7aα))-3-chloro-α-((octahydro-7,8,8-trimethyl-4,7-methano-benzofuran-2-yl)oxy)-4,5-di(phenylmethoxy)-benzeneethanamine
CAS No.:227618-77-1
Molecular Formula:C₃₄H₄₀ClNO₄
Molecular Weight:562.149
Hs Code.:

Synonyms:(2S-(2α(S*),3aα,4β,7β,7aα))-3-chloro-α-((octahydro-7,8,8-trimethyl-4,7-methano-benzofuran-2-yl)oxy)-4,5-di(phenylmethoxy)-benzeneethanamine

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Chemical Property of (2S-(2α(S*),3aα,4β,7β,7aα))-3-chloro-α-((octahydro-7,8,8-trimethyl-4,7-methano-benzofuran-2-yl)oxy)-4,5-di(phenylmethoxy)-benzeneethanamine

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Technology Process of (2S-(2α(S*),3aα,4β,7β,7aα))-3-chloro-α-((octahydro-7,8,8-trimethyl-4,7-methano-benzofuran-2-yl)oxy)-4,5-di(phenylmethoxy)-benzeneethanamine

There total 1 articles about (2S-(2α(S*),3aα,4β,7β,7aα))-3-chloro-α-((octahydro-7,8,8-trimethyl-4,7-methano-benzofuran-2-yl)oxy)-4,5-di(phenylmethoxy)-benzeneethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 7.0%

: (2S-(2α,3aα,4β,7β,7aα))-3-chloro-α-((octahydro-7,8,8-trimethyl-4,7-methano-benzofuran-2-yl)oxy)-4,5-di(phenylmethoxy)-benzeneacetonitrile

: (2S-(2α,3aα,4β,7β,7aα))-(octahydro-7,8,8-trimethyl-4,7-methano-benzofuran-2-yl) 3-chloro-4,5-di(phenylmethoxy)-benzoate

: 227618-76-0
(2S-(2α(R*),3aα,4β,7β,7aα))-3-chloro-α-((octahydro-7,8,8-trimethyl-4,7-methano-benzofuran-2-yl)oxy)-4,5-di(phenylmethoxy)-benzeneethanamine

: 227618-77-1
(2S-(2α(S*),3aα,4β,7β,7aα))-3-chloro-α-((octahydro-7,8,8-trimethyl-4,7-methano-benzofuran-2-yl)oxy)-4,5-di(phenylmethoxy)-benzeneethanamine

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether;
DOI:10.1007/PL00010225

Reference yield: 93.0%

: 501-53-1,94274-21-2
benzyl chloroformate

: 227618-77-1
(2S-(2α(S*),3aα,4β,7β,7aα))-3-chloro-α-((octahydro-7,8,8-trimethyl-4,7-methano-benzofuran-2-yl)oxy)-4,5-di(phenylmethoxy)-benzeneethanamine

: 227618-83-9
(2S-(2α(S*),3aα,4β,7β,7aα))-(phenylmethyl) N-(2-(3-chloro-4,5-di(phenylmethoxy)-phenyl)-2-((octahydro-7,8,8-trimethyl-4,7-methano-benzofuran-2-yl)oxy)-ethyl)-carbamate

Guidance literature:: With sodium hydroxide; In dichloromethane; Ambient temperature;
DOI:10.1007/PL00010225

Reference yield:

: 227618-77-1
(2S-(2α(S*),3aα,4β,7β,7aα))-3-chloro-α-((octahydro-7,8,8-trimethyl-4,7-methano-benzofuran-2-yl)oxy)-4,5-di(phenylmethoxy)-benzeneethanamine

: 227619-06-9
(R)-5-(2-(acetylmethylamino)-1-hydroxyethyl)-3-chloro-1,2-phenylene diacetate

Guidance literature:: Multi-step reaction with 5 steps

1: 93 percent / aq. NaOH / CH₂Cl₂ / Ambient temperature

2: 63 percent / LDA / tetrahydrofuran

3: 80 percent / HCl, MeOH / diethyl ether / Ambient temperature

4: 74 percent / H₂, HCl / 10 percent Pd/C / methanol; diethyl ether / 3000.24 Torr

5: 68 percent / NaHCO₃ / H₂O; CHCl₃

With hydrogenchloride; methanol; sodium hydroxide; hydrogen; sodium hydrogencarbonate; lithium diisopropyl amide; palladium on activated charcoal; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; chloroform; water;
DOI:10.1007/PL00010225