(2S-(2α(S*),3aα,4β,7β,7aα))-(phenylmethyl) N-(2-(3-chloro-4,5-di(phenylmethoxy)-phenyl)-2-((octahydro-7,8,8-trimethyl-4,7-methano-benzofuran-2-yl)oxy)-ethyl)-N-methylcarbamate

Base Information

Chemical Name:(2S-(2α(S*),3aα,4β,7β,7aα))-(phenylmethyl) N-(2-(3-chloro-4,5-di(phenylmethoxy)-phenyl)-2-((octahydro-7,8,8-trimethyl-4,7-methano-benzofuran-2-yl)oxy)-ethyl)-N-methylcarbamate
CAS No.:227618-87-3
Molecular Formula:C₄₃H₄₈ClNO₆
Molecular Weight:710.31
Hs Code.:

(2S-(2α(S*),3aα,4β,7β,7aα))-(phenylmethyl) N-(2-(3-chloro-4,5-di(phenylmethoxy)-phenyl)-2-((octahydro-7,8,8-trimethyl-4,7-methano-benzofuran-2-yl)oxy)-ethyl)-N-methylcarbamate

Synonyms:(2S-(2α(S*),3aα,4β,7β,7aα))-(phenylmethyl) N-(2-(3-chloro-4,5-di(phenylmethoxy)-phenyl)-2-((octahydro-7,8,8-trimethyl-4,7-methano-benzofuran-2-yl)oxy)-ethyl)-N-methylcarbamate

Suppliers and Price of (2S-(2α(S*),3aα,4β,7β,7aα))-(phenylmethyl) N-(2-(3-chloro-4,5-di(phenylmethoxy)-phenyl)-2-((octahydro-7,8,8-trimethyl-4,7-methano-benzofuran-2-yl)oxy)-ethyl)-N-methylcarbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (2S-(2α(S*),3aα,4β,7β,7aα))-(phenylmethyl) N-(2-(3-chloro-4,5-di(phenylmethoxy)-phenyl)-2-((octahydro-7,8,8-trimethyl-4,7-methano-benzofuran-2-yl)oxy)-ethyl)-N-methylcarbamate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (2S-(2α(S*),3aα,4β,7β,7aα))-(phenylmethyl) N-(2-(3-chloro-4,5-di(phenylmethoxy)-phenyl)-2-((octahydro-7,8,8-trimethyl-4,7-methano-benzofuran-2-yl)oxy)-ethyl)-N-methylcarbamate

There total 4 articles about (2S-(2α(S*),3aα,4β,7β,7aα))-(phenylmethyl) N-(2-(3-chloro-4,5-di(phenylmethoxy)-phenyl)-2-((octahydro-7,8,8-trimethyl-4,7-methano-benzofuran-2-yl)oxy)-ethyl)-N-methylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 227618-83-9
(2S-(2α(S*),3aα,4β,7β,7aα))-(phenylmethyl) N-(2-(3-chloro-4,5-di(phenylmethoxy)-phenyl)-2-((octahydro-7,8,8-trimethyl-4,7-methano-benzofuran-2-yl)oxy)-ethyl)-carbamate

: 74-88-4
methyl iodide

: 227618-87-3
(2S-(2α(S*),3aα,4β,7β,7aα))-(phenylmethyl) N-(2-(3-chloro-4,5-di(phenylmethoxy)-phenyl)-2-((octahydro-7,8,8-trimethyl-4,7-methano-benzofuran-2-yl)oxy)-ethyl)-N-methylcarbamate

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran;
DOI:10.1007/PL00010225

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 227618-87-3
(2S-(2α(S*),3aα,4β,7β,7aα))-(phenylmethyl) N-(2-(3-chloro-4,5-di(phenylmethoxy)-phenyl)-2-((octahydro-7,8,8-trimethyl-4,7-methano-benzofuran-2-yl)oxy)-ethyl)-N-methylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / aq. NaOH / CH₂Cl₂ / Ambient temperature

2: 63 percent / LDA / tetrahydrofuran

With sodium hydroxide; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane;
DOI:10.1007/PL00010225

Reference yield:

: (2S-(2α,3aα,4β,7β,7aα))-3-chloro-α-((octahydro-7,8,8-trimethyl-4,7-methano-benzofuran-2-yl)oxy)-4,5-di(phenylmethoxy)-benzeneacetonitrile

: 227618-87-3
(2S-(2α(S*),3aα,4β,7β,7aα))-(phenylmethyl) N-(2-(3-chloro-4,5-di(phenylmethoxy)-phenyl)-2-((octahydro-7,8,8-trimethyl-4,7-methano-benzofuran-2-yl)oxy)-ethyl)-N-methylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: 25 percent / LiAlH₄ / diethyl ether

2: 93 percent / aq. NaOH / CH₂Cl₂ / Ambient temperature

3: 63 percent / LDA / tetrahydrofuran

With sodium hydroxide; lithium aluminium tetrahydride; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1007/PL00010225