Diindeno[1,2,3-cd:1',2',3'-lm]perylene

Base Information

• Chemical Name: Diindeno[1,2,3-cd:1',2',3'-lm]perylene
• CAS No.: 188-94-3
• Molecular Formula: C32H16
• Molecular Weight: 400.479
• European Community (EC) Number: 205-875-4
• NSC Number: 87529
• UNII: TQA4WPL7Y8
• DSSTox Substance ID: DTXSID40172139
• Nikkaji Number: J5.875K
• Wikipedia: Diindenoperylene
• Wikidata: Q3027899
• Mol file: 188-94-3.mol

Synonyms:diindenoperylene

Chemical Property of Diindeno[1,2,3-cd:1',2',3'-lm]perylene

Chemical Property:

• Appearance/Colour: orange solid
• Melting Point: >400 °C
• Flash Point: 6 °C
• PSA: 0.00000
• Density: 1.467 g/cm³
• LogP: 9.03200
• Storage Temp.: -20°C
• XLogP3: 3.1
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 0
• Exact Mass: 400.125200510
• Heavy Atom Count: 32
• Complexity: 1450

Purity/Quality:

99% ^*data from raw suppliers

diindeno[1,2,3-cd:1'',2'',3''-lm]perylene 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s): FXn
• Hazard Codes: F,Xn
• Statements: 11-38-48/20-63-65-67
• Safety Statements: 36/37-62

MSDS Files:

SDS file from LookChem

Useful:

• Chemical Classes: Other Classes -> Polycyclic Aromatic Hydrocarbons
• Canonical SMILES: C1=CC2=C3C=CC4=C5C=CC6=C7C=CC=CC7=C8C6=C5C(=C9C4=C3C(=C2C=C1)C=C9)C=C8

Technology Process of Diindeno[1,2,3-cd:1',2',3'-lm]perylene

There total 6 articles about Diindeno[1,2,3-cd:1',2',3'-lm]perylene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.7%

fluoranthene (206-44-0) → Diindeno<1,2,3-c,d:1',2',3'-lm>perylene (188-94-3)

Guidance literature:

With sodium amide; In N,N-dimethyl acetamide; at 162.5 - 165.5 ℃; for 10h; Temperature; Solvent; Inert atmosphere;

Reference yield:

→ Diindeno<1,2,3-c,d:1',2',3'-lm>perylene (188-94-3)

Guidance literature:

With sodium amide; decalin; at 200 ℃;

Reference yield:

PERYLENE (198-55-0) + benzene (71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1) → Diindeno<1,2,3-c,d:1',2',3'-lm>perylene (188-94-3)

Guidance literature:

With aluminium trichloride; zuletzt bei Siedetemperatur;

DOI:10.1007/BF00899529 DOI:10.1007/BF00913855

upstream raw materials:

fluoranthene

PERYLENE

benzene

decalin

Refernces

• 1、 Zinke et al.. "-". . p. 1497,1501. Retrieved 1952.
• 2、 Kubozono, Y.,Ata, M.,Gondo, Y.. "Electronic structure of diindenoperylene radical anion". . p. 57 - 59. Retrieved 1990.