(+/-)-2-<2-Methoxy-4-(methylsulfinyl)phenyl>-5-methylimidazo-1H-<4,5-b>pyridin

Base Information

Chemical Name:(+/-)-2-<2-Methoxy-4-(methylsulfinyl)phenyl>-5-methylimidazo-1H-<4,5-b>pyridin
CAS No.:144563-54-2
Molecular Formula:C₁₅H₁₅N₃O₂S
Molecular Weight:301.369
Hs Code.:

Synonyms:(+/-)-2-<2-Methoxy-4-(methylsulfinyl)phenyl>-5-methylimidazo-1H-<4,5-b>pyridin

Suppliers and Price of (+/-)-2-<2-Methoxy-4-(methylsulfinyl)phenyl>-5-methylimidazo-1H-<4,5-b>pyridin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)-2-<2-Methoxy-4-(methylsulfinyl)phenyl>-5-methylimidazo-1H-<4,5-b>pyridin

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Technology Process of (+/-)-2-<2-Methoxy-4-(methylsulfinyl)phenyl>-5-methylimidazo-1H-<4,5-b>pyridin

There total 3 articles about (+/-)-2-<2-Methoxy-4-(methylsulfinyl)phenyl>-5-methylimidazo-1H-<4,5-b>pyridin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 144563-52-0
2-<2-Methoxy-4-(methylthio)phenyl>-5-methylimidazo-1H-<4,5-b>pyridin

: 144563-54-2
(+/-)-2-<2-Methoxy-4-(methylsulfinyl)phenyl>-5-methylimidazo-1H-<4,5-b>pyridin

Guidance literature:: With dihydrogen peroxide; In acetic acid; for 6h; Ambient temperature;
DOI:10.1002/ardp.19923250918

Reference yield:

: 33259-72-2
2,3-diamino-6-methyl-pyridine

: 144563-54-2
(+/-)-2-<2-Methoxy-4-(methylsulfinyl)phenyl>-5-methylimidazo-1H-<4,5-b>pyridin

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / POCl₃ / a) r.t., 30 min, 2) reflux, 4.5 h

2: 75 percent / 30percent H₂O₂ / acetic acid / 6 h / Ambient temperature

With dihydrogen peroxide; trichlorophosphate; In acetic acid;
DOI:10.1002/ardp.19923250918

Reference yield:

: 21901-29-1
6-amino-5-nitro-2-picoline

: 144563-54-2
(+/-)-2-<2-Methoxy-4-(methylsulfinyl)phenyl>-5-methylimidazo-1H-<4,5-b>pyridin

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / H₂ / 10percent Pd/C / ethyl acetate / 1.5 h / 2625.2 Torr / Ambient temperature

2: 71 percent / POCl₃ / a) r.t., 30 min, 2) reflux, 4.5 h

3: 75 percent / 30percent H₂O₂ / acetic acid / 6 h / Ambient temperature

With hydrogen; dihydrogen peroxide; trichlorophosphate; palladium on activated charcoal; In acetic acid; ethyl acetate;
DOI:10.1002/ardp.19923250918