butyric acid (1R,2S)-2-(1-phenyl-1H-tetrazol-5-ylsulfanylmethyl)cyclopropyl methyl ester

Base Information

Chemical Name:butyric acid (1R,2S)-2-(1-phenyl-1H-tetrazol-5-ylsulfanylmethyl)cyclopropyl methyl ester
CAS No.:934503-08-9
Molecular Formula:C₁₆H₂₀N₄O₂S
Molecular Weight:332.426
Hs Code.:

Synonyms:butyric acid (1R,2S)-2-(1-phenyl-1H-tetrazol-5-ylsulfanylmethyl)cyclopropyl methyl ester

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Chemical Property of butyric acid (1R,2S)-2-(1-phenyl-1H-tetrazol-5-ylsulfanylmethyl)cyclopropyl methyl ester

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Technology Process of butyric acid (1R,2S)-2-(1-phenyl-1H-tetrazol-5-ylsulfanylmethyl)cyclopropyl methyl ester

There total 1 articles about butyric acid (1R,2S)-2-(1-phenyl-1H-tetrazol-5-ylsulfanylmethyl)cyclopropyl methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 133494-56-1
cis-(1R,2S)-1-butyryloxymethyl-2-hydroxymethylcyclopropane

: 86-93-1
1-Phenyl-1H-tetrazole-5-thiol

: 934503-08-9
butyric acid (1R,2S)-2-(1-phenyl-1H-tetrazol-5-ylsulfanylmethyl)cyclopropyl methyl ester

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 20 ℃; for 18h;
DOI:10.1016/j.tet.2007.01.007

Reference yield: 93.0%

: 934503-08-9
butyric acid (1R,2S)-2-(1-phenyl-1H-tetrazol-5-ylsulfanylmethyl)cyclopropyl methyl ester

: 934503-10-3
butyric acid (1R,2S)-2-(1-phenyl-1H-tetrazol-5-sulfonylmethyl)cyclopropyl methyl ester

Guidance literature:: With ammonium molybdate tetrahydrate; dihydrogen peroxide; In tetrahydrofuran; at 20 ℃; for 2h;
DOI:10.1016/j.tet.2007.01.007

Reference yield:

: 934503-08-9
butyric acid (1R,2S)-2-(1-phenyl-1H-tetrazol-5-ylsulfanylmethyl)cyclopropyl methyl ester

: 934503-18-1
5-{7-[(1S,2R)-2-((17R,18R)-17-methoxy-18-methylhexatriacontyl)cyclopropyl]heptylsulfanyl}-1-phenyl-1H-tetrazole

Guidance literature:: Multi-step reaction with 8 steps

1: 93 percent / ammonium heptamolybdate(VI) tetrahydrate; aq. hydrogen peroxide / tetrahydrofuran; various solvent(s) / 2 h / 20 °C

2: 74 percent / lithium hexamethyldisilazide / tetrahydrofuran / 16 h / 20 °C

3: 80 percent / 2,4,6-triisopropylbenzene sulfonylhydrazide / tetrahydrofuran / 20 h / 50 °C

4: 85 percent / potassium carbonate / methanol; tetrahydrofuran / 4 h / 45 °C

5: 76 percent / pyridinium chlorochromate / CH₂Cl₂ / 3 h / 20 °C

6: 74 percent / lithium hexamethyldisilazide / tetrahydrofuran / 2 h / 20 °C

7: 80 percent / 2,4,6-triisopropyl sulfonylhydrazide / tetrahydrofuran / 52 °C

8: 88 percent / potassium carbonate / tetrahydrofuran; acetone / 21 h / 20 - 40 °C

With ammonium molybdate tetrahydrate; 2,4,6-triisopropyl sulfonylhydrazide; trisylhydrazine; dihydrogen peroxide; potassium carbonate; pyridinium chlorochromate; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; dichloromethane; acetone; 2: Julia-Kocienski reaction / 6: Julia-Kocienski reaction;
DOI:10.1016/j.tet.2007.01.007