di(2-methoxyphenyl)sulfurdiimine

Base Information

• Chemical Name: di(2-methoxyphenyl)sulfurdiimine
• CAS No.: 19551-94-1
• Molecular Formula: C₁₄H₁₄N₂O₂S
• Molecular Weight: 274.343

Synonyms:di(2-methoxyphenyl)sulfurdiimine

Chemical Property of di(2-methoxyphenyl)sulfurdiimine

Chemical Property:

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Technology Process of di(2-methoxyphenyl)sulfurdiimine

There total 3 articles about di(2-methoxyphenyl)sulfurdiimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

N?sulfinyl?2?methoxyaniline (17419-98-6) → di(2-methoxyphenyl)sulfurdiimine (19551-94-1)

Guidance literature:

With Ta(N^tBu)(CH₂CMe₂Ph)₃/SiO₂; In n-heptane; for 24h; Inert atmosphere; Schlenk technique; Reflux;

DOI:10.1021/om4001499

Reference yield:

N?sulfinyl?2?methoxyaniline (17419-98-6) + N,N-dimethyl-formamide (68-12-2,33513-42-7) → N.N-Dimethyl-N'-<2-methoxy-phenyl>-formamidin (2103-48-2) + di(2-methoxyphenyl)sulfurdiimine (19551-94-1)

Guidance literature:

With (MesN)2-Mo(CH₂CMe₂Ph)2; In n-heptane; for 20h; Reflux; Inert atmosphere;

DOI:10.1016/j.mencom.2009.05.019

Reference yield:

→ di(2-methoxyphenyl)sulfurdiimine (19551-94-1)

Guidance literature:

Thionyl-o-anisidin, Na-Staub, sd. Toluol;

upstream raw materials:

N?sulfinyl?2?methoxyaniline

N,N-dimethyl-formamide

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