LUF₅₇₂₄

Base Information

• Chemical Name: LUF₅₇₂₄
• CAS No.: 15850-23-4
• Molecular Formula: C₁₆H₁₁N₃O₃S
• Molecular Weight: 325.348
• Mol file: 15850-23-4.mol

Synonyms:LUF₅₇₂₄

Chemical Property of LUF₅₇₂₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of LUF₅₇₂₄

There total 2 articles about LUF₅₇₂₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

2-amino-4-phenyl-thiazole hydrobromide (34161-31-4) + 4-nitro-benzoyl chloride (122-04-3) → LUF5724 (15850-23-4)

Guidance literature:

With triethylamine; In 1,4-dioxane; Heating;

DOI:10.1016/S0960-894X(01)00356-0

Reference yield:

→ LUF5724 (15850-23-4)

Guidance literature:

Acyl. des Amins;

Reference yield:

LUF5724 (15850-23-4) → 2-p-nitrophenyl-5-phenylthiazolo<3,2-b>-s-triazole (54294-13-2)

Guidance literature:

Multi-step reaction with 3 steps

1: PCl₅ / 1.5 h / 130 °C

2: sodium azide, sodium acetate / acetone; H₂O / 8 h

3: 44 percent / decahydronaphthalene / 2 h / Heating

With sodium azide; phosphorus pentachloride; sodium acetate; In water; acetone; decalin;

upstream raw materials:

2-amino-4-phenyl-thiazole hydrobromide

4-nitro-benzoyl chloride

Downstream raw materials:

1-(4-phenylthiazol-2-yl)-5-p-nitrophenyltetrazole

2-p-nitrophenyl-5-phenylthiazolo<3,2-b>-s-triazole