Technology Process of C26H19BO7
There total 5 articles about C26H19BO7 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C26H19BO8;
With
dichloro-acetic acid; hydrogen;
platinum(IV) oxide;
In
ethyl acetate;
at 20 ℃;
for 2h;
With
air; sodium hydrogencarbonate;
In
tetrahydrofuran;
DOI:10.1071/ch99151
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 32 mg / AlCl3 / CH2Cl2 / 16 h / 20 °C
2.1: 98 percent / p-TsOH / CH2Cl2 / 16 h / 20 °C
3.1: dichloroacetic acid; H2 / Adams catalyst / ethyl acetate / 2 h / 20 °C
3.2: 98 percent / air; sat. aq. NaHCO3 / tetrahydrofuran
With
dichloro-acetic acid; aluminium trichloride; hydrogen; toluene-4-sulfonic acid;
platinum(IV) oxide;
In
dichloromethane; ethyl acetate;
1.1: demethylation / 2.1: Esterification / 3.1: Catalytic hydrogenation / 3.2: Oxidation;
DOI:10.1071/ch99151
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: 98 percent / p-TsOH / CH2Cl2 / 16 h / 20 °C
2.1: dichloroacetic acid; H2 / Adams catalyst / ethyl acetate / 2 h / 20 °C
2.2: 98 percent / air; sat. aq. NaHCO3 / tetrahydrofuran
With
dichloro-acetic acid; hydrogen; toluene-4-sulfonic acid;
platinum(IV) oxide;
In
dichloromethane; ethyl acetate;
1.1: Esterification / 2.1: Catalytic hydrogenation / 2.2: Oxidation;
DOI:10.1071/ch99151