2-(4-fluorophenyl)methylamino-N-(methylamino)(methylthio)methylene-3-pyridinecarboxamide

Base Information

Chemical Name:2-(4-fluorophenyl)methylamino-N-(methylamino)(methylthio)methylene-3-pyridinecarboxamide
CAS No.:58537-02-3
Molecular Formula:C₁₆H₁₇FN₄OS
Molecular Weight:332.402
Hs Code.:

Synonyms:2-(4-fluorophenyl)methylamino-N-(methylamino)(methylthio)methylene-3-pyridinecarboxamide

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Chemical Property of 2-(4-fluorophenyl)methylamino-N-(methylamino)(methylthio)methylene-3-pyridinecarboxamide

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Technology Process of 2-(4-fluorophenyl)methylamino-N-(methylamino)(methylthio)methylene-3-pyridinecarboxamide

There total 6 articles about 2-(4-fluorophenyl)methylamino-N-(methylamino)(methylthio)methylene-3-pyridinecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 41306-45-0
N,S-dimethylisothiourea hydroiodide

: 53914-11-7
2-<(4-fluorophenyl)methyl>-2H-pyrido<2,3-d><1,3>oxazine-2,4-(1H)-dione

: 58537-02-3
2-(4-fluorophenyl)methylamino-N-(methylamino)(methylthio)methylene-3-pyridinecarboxamide

Guidance literature:: With sodium carbonate; In acetonitrile; for 1h; Heating;

Reference yield:

: 2942-59-8
2-chloronicotinic acid

: 58537-02-3
2-(4-fluorophenyl)methylamino-N-(methylamino)(methylthio)methylene-3-pyridinecarboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: 1) potassium carbonate, 2) Cu / 1) water, RT, 2) dimethylformamide, reflux, 8 h

2: 62 percent / sodium carbonate / H₂O; benzene / 18 h / Ambient temperature

3: 75 percent / sodium carbonate / acetonitrile / 1 h / Heating

With copper; sodium carbonate; potassium carbonate; In water; acetonitrile; benzene;

Reference yield:

: 97484-91-8
2-<(4-fluorophenyl)methylamino>-3-pyridinecarboxylic acid

: 58537-02-3
2-(4-fluorophenyl)methylamino-N-(methylamino)(methylthio)methylene-3-pyridinecarboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: 62 percent / sodium carbonate / H₂O; benzene / 18 h / Ambient temperature

2: 75 percent / sodium carbonate / acetonitrile / 1 h / Heating

With sodium carbonate; In water; acetonitrile; benzene;