Pyridine, 2-benzylamino-, hydrochloride

Base Information

• Chemical Name: Pyridine, 2-benzylamino-, hydrochloride
• CAS No.: 67465-04-7
• Molecular Formula: C12H12N2•ClH
• Molecular Weight: 220.70
• DSSTox Substance ID: DTXSID70217800
• ChEMBL ID: CHEMBL1372868

Synonyms:Pyridine, 2-benzylamino-, hydrochloride;2-Bap hydrochloride;67465-04-7;2-Benzylaminopyridine hydrochloride;N-benzylpyridin-2-amine;hydrochloride;Benzylamine, N-(2-pyridyl)-, hydrochloride;BIDD:GT0704;SCHEMBL4696844;CHEMBL1372868;DTXSID70217800;LS-130286

Chemical Property of Pyridine, 2-benzylamino-, hydrochloride

Chemical Property:

• Vapor Pressure: 0.000291mmHg at 25°C
• Boiling Point: 321.8°Cat760mmHg
• Flash Point: 148.4°C
• PSA: 24.92000
• Density: g/cm³
• LogP: 4.37070
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 3
• Exact Mass: 220.0767261
• Heavy Atom Count: 15
• Complexity: 152

Purity/Quality:

99% ^*data from raw suppliers

BENZYL-PYRIDIN-2-YL-AMINE DIHYDROCHLORIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)CNC2=CC=CC=N2.Cl

Technology Process of Pyridine, 2-benzylamino-, hydrochloride

There total 2 articles about Pyridine, 2-benzylamino-, hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-amino-1-benzylpyridinium chloride (141206-63-5) → 2-aminopyridine (504-29-0) + benzyl chloride (100-44-7) + 1,1'-(1,2-ethanediyl)bisbenzene (103-29-7) + 2-benzylaminopyridine hydrochloride (67465-04-7) + 2-(N,N-dibenzylamino)pyridine hydrochloride + 2-benzylamino-5-benzylpyridine hydrochloride

Guidance literature:

In neat (no solvent); at 235 - 250 ℃; for 2h; Product distribution; Mechanism; variation of time;

Reference yield:

1-benzyl-2-benzylaminopyridinium chloride → 2-aminopyridine (504-29-0) + 2-amino-1-benzylpyridinium chloride (141206-63-5) + 2-amino-5-benzylpyridine (98477-40-8) + 2-benzylaminopyridine hydrochloride (67465-04-7) + 2-(N,N-dibenzylamino)pyridine hydrochloride + 2-benzylamino-5-benzylpyridine hydrochloride

Guidance literature:

In neat (no solvent); at 250 ℃; for 2h; Product distribution; Mechanism; variation of time;

Reference yield:

sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate (79060-88-1) + 2-benzylaminopyridine hydrochloride (67465-04-7) → 2-(benzylamino)pyridinium tetrakis(3,5-bis(trifluoromethyl)phenyl)borate

Guidance literature:

In ethanol; for 0.5h;

DOI:10.1021/jo991372x

upstream raw materials:

2-amino-1-benzylpyridinium chloride

Downstream raw materials:

2-aminopyridine

2-amino-5-benzylpyridine

2-Benzylamino-5-benzylpyridine

2-(N,N-dibenzylamino)pyridine

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