(5S)-6-{[tert-butyl(diphenyl)silyl]oxy}-5-[(3-methylbutyl)amino]hexan-1-ol

Base Information

Chemical Name:(5S)-6-{[tert-butyl(diphenyl)silyl]oxy}-5-[(3-methylbutyl)amino]hexan-1-ol
CAS No.:1374138-01-8
Molecular Formula:C₂₇H₄₃NO₂Si
Molecular Weight:441.729
Hs Code.:

Synonyms:(5S)-6-{[tert-butyl(diphenyl)silyl]oxy}-5-[(3-methylbutyl)amino]hexan-1-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (5S)-6-{[tert-butyl(diphenyl)silyl]oxy}-5-[(3-methylbutyl)amino]hexan-1-ol

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Technology Process of (5S)-6-{[tert-butyl(diphenyl)silyl]oxy}-5-[(3-methylbutyl)amino]hexan-1-ol

There total 7 articles about (5S)-6-{[tert-butyl(diphenyl)silyl]oxy}-5-[(3-methylbutyl)amino]hexan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₂H₃₃NO₂Si*ClH

: 590-86-3
isovaleraldehyde

: 1374138-01-8
(5S)-6-{[tert-butyl(diphenyl)silyl]oxy}-5-[(3-methylbutyl)amino]hexan-1-ol

Guidance literature:: C₂₂H₃₃NO₂Si*ClH; isovaleraldehyde; With acetic acid; In methanol; at 20 ℃; for 0.5h;

With methanol; sodium cyanoborohydride; at 20 ℃;

Reference yield:

: 2389-48-2
N-ε-tert-butoxycarbonyl-L-lysine methyl ester hydrochloride

: 1374138-01-8
(5S)-6-{[tert-butyl(diphenyl)silyl]oxy}-5-[(3-methylbutyl)amino]hexan-1-ol

Guidance literature:: Multi-step reaction with 7 steps

1.1: triethylamine / dichloromethane / 20 °C

2.1: lithium borohydride / tetrahydrofuran / 2 h / 0 - 50 °C

2.2: 0 - 20 °C

3.1: 1H-imidazole / dichloromethane / 0 - 20 °C

4.1: sodium bromate; ruthenium(IV) oxide hydrate / ethyl acetate; water / 20 - 55 °C

5.1: water; sodium tetrahydroborate / isopropyl alcohol / 20 °C

6.1: hydrogenchloride / 1,4-dioxane / 1 h / 20 °C

7.1: acetic acid / methanol / 0.5 h / 20 °C

7.2: 20 °C

With 1H-imidazole; hydrogenchloride; sodium bromate; sodium tetrahydroborate; lithium borohydride; ruthenium(IV) oxide hydrate; water; acetic acid; triethylamine; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; ethyl acetate; isopropyl alcohol;

Reference yield:

: 85535-55-3
(S)-di-tert-butyl (6-hydroxyhexane-1,5-diyl)dicarbamate

: 1374138-01-8
(5S)-6-{[tert-butyl(diphenyl)silyl]oxy}-5-[(3-methylbutyl)amino]hexan-1-ol

Guidance literature:: Multi-step reaction with 5 steps

1.1: 1H-imidazole / dichloromethane / 0 - 20 °C

2.1: sodium bromate; ruthenium(IV) oxide hydrate / ethyl acetate; water / 20 - 55 °C

3.1: water; sodium tetrahydroborate / isopropyl alcohol / 20 °C

4.1: hydrogenchloride / 1,4-dioxane / 1 h / 20 °C

5.1: acetic acid / methanol / 0.5 h / 20 °C

5.2: 20 °C

With 1H-imidazole; hydrogenchloride; sodium bromate; sodium tetrahydroborate; ruthenium(IV) oxide hydrate; water; acetic acid; In 1,4-dioxane; methanol; dichloromethane; water; ethyl acetate; isopropyl alcohol;