cis-2,3,4,4a,5,6,7,11c-octahydro-5α-chloro-7-<(p-methoxyphenyl)-sulfonyl>-1H-pyrido<3,2-c>carbazole

Base Information

Chemical Name:cis-2,3,4,4a,5,6,7,11c-octahydro-5α-chloro-7-<(p-methoxyphenyl)-sulfonyl>-1H-pyrido<3,2-c>carbazole
CAS No.:84960-67-8
Molecular Formula:C₂₂H₂₃ClN₂O₃S
Molecular Weight:430.955
Hs Code.:

Synonyms:cis-2,3,4,4a,5,6,7,11c-octahydro-5α-chloro-7-<(p-methoxyphenyl)-sulfonyl>-1H-pyrido<3,2-c>carbazole

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Chemical Property of cis-2,3,4,4a,5,6,7,11c-octahydro-5α-chloro-7-<(p-methoxyphenyl)-sulfonyl>-1H-pyrido<3,2-c>carbazole

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Technology Process of cis-2,3,4,4a,5,6,7,11c-octahydro-5α-chloro-7-<(p-methoxyphenyl)-sulfonyl>-1H-pyrido<3,2-c>carbazole

There total 4 articles about cis-2,3,4,4a,5,6,7,11c-octahydro-5α-chloro-7-<(p-methoxyphenyl)-sulfonyl>-1H-pyrido<3,2-c>carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 88981-61-7
2,2,2-trichloroethyl cis-2,3,4,4a,5,6,7,11c-octahydro-5α-chloro-7-<(p-methoxyphenyl)sulfonyl>-1H-pyrido<3,2-c>carbazole-1-carboxylate

: 84960-67-8
cis-2,3,4,4a,5,6,7,11c-octahydro-5α-chloro-7-<(p-methoxyphenyl)-sulfonyl>-1H-pyrido<3,2-c>carbazole

Guidance literature:: With acetic acid; zinc; In tetrahydrofuran; water; at 20 ℃;
DOI:10.1021/ja00345a081

Reference yield:

: 80664-26-2
N-<(4-methoxyphenyl)sulfonyl>-2-methylindole-3-carboxaldehyde

: 84960-67-8
cis-2,3,4,4a,5,6,7,11c-octahydro-5α-chloro-7-<(p-methoxyphenyl)-sulfonyl>-1H-pyrido<3,2-c>carbazole

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / 4A molecular sieves

2: 50 percent / N(i-Pr)2Et / chlorobenzene / 120 °C

3: 91 percent / Zn, AcOH / tetrahydrofuran; H₂O / 20 °C

With 4 A molecular sieve; acetic acid; N-ethyl-N,N-diisopropylamine; zinc; In tetrahydrofuran; water; chlorobenzene;
DOI:10.1021/ja00345a081

Reference yield:

: 84960-65-6
((E)-5-Chloro-pent-4-enyl)-[1-[1-(4-methoxy-benzenesulfonyl)-2-methyl-1H-indol-3-yl]-meth-(E)-ylidene]-amine

: 84960-67-8
cis-2,3,4,4a,5,6,7,11c-octahydro-5α-chloro-7-<(p-methoxyphenyl)-sulfonyl>-1H-pyrido<3,2-c>carbazole

Guidance literature:: Multi-step reaction with 2 steps

1: 50 percent / N(i-Pr)2Et / chlorobenzene / 120 °C

2: 91 percent / Zn, AcOH / tetrahydrofuran; H₂O / 20 °C

With acetic acid; N-ethyl-N,N-diisopropylamine; zinc; In tetrahydrofuran; water; chlorobenzene;
DOI:10.1021/ja00345a081