(S)-(-)-2-(N-propylamino)-5-methoxytetraline (+)-N-(3,5-dinitrobenzoyl)-α-phenylglycine salt

Base Information

Chemical Name:(S)-(-)-2-(N-propylamino)-5-methoxytetraline (+)-N-(3,5-dinitrobenzoyl)-α-phenylglycine salt
CAS No.:1222074-03-4
Molecular Formula:C₁₄H₂₁NO*C₁₅H₁₁N₃O₇
Molecular Weight:564.595
Hs Code.:

Synonyms:(S)-(-)-2-(N-propylamino)-5-methoxytetraline (+)-N-(3,5-dinitrobenzoyl)-α-phenylglycine salt

Suppliers and Price of (S)-(-)-2-(N-propylamino)-5-methoxytetraline (+)-N-(3,5-dinitrobenzoyl)-α-phenylglycine salt

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of (S)-(-)-2-(N-propylamino)-5-methoxytetraline (+)-N-(3,5-dinitrobenzoyl)-α-phenylglycine salt

Chemical Property:

Purity/Quality:: 98% HPLC ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (S)-(-)-2-(N-propylamino)-5-methoxytetraline (+)-N-(3,5-dinitrobenzoyl)-α-phenylglycine salt

There total 1 articles about (S)-(-)-2-(N-propylamino)-5-methoxytetraline (+)-N-(3,5-dinitrobenzoyl)-α-phenylglycine salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

: 78598-91-1,3899-07-8
2-(N-propylamino)-5-methoxytetraline

: 90761-62-9
(S)-(+)-N-(3,5-dinitrobenzoyl)-α-phenylglycine

: 1222074-03-4
(S)-(-)-2-(N-propylamino)-5-methoxytetraline (+)-N-(3,5-dinitrobenzoyl)-α-phenylglycine salt

Guidance literature:: In water; acetonitrile; at 0 - 5 ℃; Heating; Resolution of racemate;

Reference yield: 98.0%

: 1222074-03-4
(S)-(-)-2-(N-propylamino)-5-methoxytetraline (+)-N-(3,5-dinitrobenzoyl)-α-phenylglycine salt

: 101403-24-1,3899-07-8
(S)-(5-methoxy-1,2,3,4-tetrahydro-naphthalen-2-yl)-propylamine hydrochloride

Guidance literature:: With potassium carbonate; In toluene; at 60 ℃;

Reference yield:

: 1222074-03-4
(S)-(-)-2-(N-propylamino)-5-methoxytetraline (+)-N-(3,5-dinitrobenzoyl)-α-phenylglycine salt

: 99755-59-6,112835-48-0
rotigotine

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / toluene / 60 °C

2.1: hydrogen bromide / acetic acid / 3 h / Reflux

2.2: pH 12.5

2.3: pH 9 - 9.5

3.1: sodium hydrogencarbonate / acetonitrile / 9 h / Reflux

3.2: pH 1 - 2

3.3: pH 7 - 7.5

With hydrogen bromide; sodium hydrogencarbonate; potassium carbonate; In acetic acid; toluene; acetonitrile;