methoxymethyl benzylpenicillinate 1,1-dioxide

Base Information

• Chemical Name: methoxymethyl benzylpenicillinate 1,1-dioxide
• CAS No.: 121002-98-0
• Molecular Formula: C₁₈H₂₂N₂O₇S
• Molecular Weight: 410.448
• Mol file: 121002-98-0.mol

Synonyms:methoxymethyl benzylpenicillinate 1,1-dioxide

Chemical Property of methoxymethyl benzylpenicillinate 1,1-dioxide

Chemical Property:

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Technology Process of methoxymethyl benzylpenicillinate 1,1-dioxide

There total 1 articles about methoxymethyl benzylpenicillinate 1,1-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

benzylpenicillin 1,1-dioxide (18598-31-7) + chloromethyl methyl ether (107-30-2) → methoxymethyl benzylpenicillinate 1,1-dioxide (121002-98-0)

Guidance literature:

With triethylamine; In dichloromethane; at 0 ℃; for 0.5h;

DOI:10.1039/P19880002813

Reference yield: 47.0%

methoxymethyl benzylpenicillinate 1,1-dioxide (121002-98-0) → (2R,3S)-1-(1-methoxymethoxycarbonyl-2-methylprop-1-enyl)-4-oxo-3-phenylacetamidoazetidine-2-sulphinic acid (121002-99-1)

Guidance literature:

With 2,6-dichloro-benzonitrile; In dichloromethane;

DOI:10.1039/P19880002813

upstream raw materials:

benzylpenicillin 1,1-dioxide

chloromethyl methyl ether

Downstream raw materials:

(2R,3S)-1-(1-methoxymethoxycarbonyl-2-methylprop-1-enyl)-4-oxo-3-phenylacetamidoazetidine-2-sulphinic acid