4-Thia-1-azabicyclo[3.2.0]heptane-2-carboxylic acid, 3,3-dimethyl-7-oxo-6-[(phenylacetyl)amino]- (2S,5R,6R)-, 4,4-dioxide

Base Information Edit

Chemical Name:4-Thia-1-azabicyclo[3.2.0]heptane-2-carboxylic acid, 3,3-dimethyl-7-oxo-6-[(phenylacetyl)amino]- (2S,5R,6R)-, 4,4-dioxide
CAS No.:18598-31-7
Molecular Formula:C16H18N2O6S
Molecular Weight:366.395
Hs Code.:
Mol file:18598-31-7.mol

Synonyms:

Suppliers and Price of 4-Thia-1-azabicyclo[3.2.0]heptane-2-carboxylic acid, 3,3-dimethyl-7-oxo-6-[(phenylacetyl)amino]- (2S,5R,6R)-, 4,4-dioxide

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4-Thia-1-azabicyclo[3.2.0]heptane-2-carboxylic acid, 3,3-dimethyl-7-oxo-6-[(phenylacetyl)amino]- (2S,5R,6R)-, 4,4-dioxide Edit

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-Thia-1-azabicyclo[3.2.0]heptane-2-carboxylic acid, 3,3-dimethyl-7-oxo-6-[(phenylacetyl)amino]- (2S,5R,6R)-, 4,4-dioxide

There total 7 articles about 4-Thia-1-azabicyclo[3.2.0]heptane-2-carboxylic acid, 3,3-dimethyl-7-oxo-6-[(phenylacetyl)amino]- (2S,5R,6R)-, 4,4-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 113-98-4
Penicillin G potassium

: 18598-31-7
benzylpenicillin 1,1-dioxide

Guidance literature:: With potassium permanganate; phosphoric acid; In water; at 0 - 10 ℃; for 1h; pH mantained at 7.2 with 2percent NaOH;

Reference yield:

: 101522-53-6
1,1-dioxo-6β-(2-phenyl-acetylamino)-1λ⁶-penicillanic acid benzyl ester

: 18598-31-7
benzylpenicillin 1,1-dioxide

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; under 2585.7 Torr;
DOI:10.1021/jo01051a061

Reference yield:

: 1254-56-4
benzyl (2S,5R,6R)-3,3-dimethyl-7-oxo-6-(2-phenylacetamido)-4-thia-1-azabicyclo[3.2.0]heptane-2-carboxylate

: 18598-31-7
benzylpenicillin 1,1-dioxide

Guidance literature:: Multi-step reaction with 2 steps

1: aq. KMnO₄, H₂O₂ / acetic acid

2: H₂ / Pd-C / methanol / 2585.7 Torr

With potassium permanganate; hydrogen; dihydrogen peroxide; palladium on activated charcoal; In methanol; acetic acid;
DOI:10.1021/jo01051a061