methyl 2-((1-(((tert-butyl(dimethyl)silyl)oxy)methyl)prop-2-enyl)oxy)-6-hydroxybenzoate

Base Information

• Chemical Name: methyl 2-((1-(((tert-butyl(dimethyl)silyl)oxy)methyl)prop-2-enyl)oxy)-6-hydroxybenzoate
• CAS No.: 745079-05-4
• Molecular Formula: C₁₈H₂₈O₅Si
• Molecular Weight: 352.503

Synonyms:methyl 2-((1-(((tert-butyl(dimethyl)silyl)oxy)methyl)prop-2-enyl)oxy)-6-hydroxybenzoate

Chemical Property of methyl 2-((1-(((tert-butyl(dimethyl)silyl)oxy)methyl)prop-2-enyl)oxy)-6-hydroxybenzoate

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Technology Process of methyl 2-((1-(((tert-butyl(dimethyl)silyl)oxy)methyl)prop-2-enyl)oxy)-6-hydroxybenzoate

There total 2 articles about methyl 2-((1-(((tert-butyl(dimethyl)silyl)oxy)methyl)prop-2-enyl)oxy)-6-hydroxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

methyl 2,6-dihydroxybenzoate (2150-45-0) + 1-((tert-butyldimethylsilyl)oxy)but-3-en-2-ol (136917-96-9,136984-28-6,119125-28-9) → methyl 2-((1-(((tert-butyl(dimethyl)silyl)oxy)methyl)prop-2-enyl)oxy)-6-hydroxybenzoate (745079-05-4)

Guidance literature:

With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 0 - 20 ℃; for 16h;

Reference yield: 24.0%

methyl 2,6-dihydroxybenzoate (2150-45-0) + 1-((tert-butyldimethylsilyl)oxy)but-3-en-2-ol (136917-96-9,136984-28-6,119125-28-9) + diethylazodicarboxylate (1972-28-7,218603-74-8) → methyl 2-((1-(((tert-butyl(dimethyl)silyl)oxy)methyl)prop-2-enyl)oxy)-6-hydroxybenzoate (745079-05-4)

Guidance literature:

With triphenylphosphine; In tetrahydrofuran;

Reference yield: 19.0%

methyl 2-((1-(((tert-butyl(dimethyl)silyl)oxy)methyl)prop-2-enyl)oxy)-6-hydroxybenzoate (745079-05-4) + 5-(3-iodo-phenyl)-isoxazole-3-carboxylic acid methyl ester (609848-44-4) → methyl 5-(3-((1E)-4-((tert-butyl(dimethyl)silyl)oxy)-3-(3-hydroxy-2-(methoxycarbonyl)phenoxy)but-1-enyl)phenyl)isoxazole-3-carboxylate (745079-06-5)

Guidance literature:

With triethylamine; tris-(o-tolyl)phosphine; palladium diacetate; at 80 ℃; for 3h;

upstream raw materials:

methyl 2,6-dihydroxybenzoate

1-((tert-butyldimethylsilyl)oxy)but-3-en-2-ol

diethylazodicarboxylate

Downstream raw materials:

methyl 5-(3-((1E)-4-((tert-butyl(dimethyl)silyl)oxy)-3-(3-hydroxy-2-(methoxycarbonyl)phenoxy)but-1-enyl)phenyl)isoxazole-3-carboxylate

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