(CH₃)3CC₆H₄C(NC₆H₃(CH(CH₃)2)2)2^(1-)*Pb⁽²⁺⁾*O₃SCF₃^(1-)*OC₄H₈=((CH₃)3CC₆H₄C(NC₆H₃(CH(CH₃)2)2)2)Pb(O₃SCF₃)(OC₄H₈)

Base Information

• Chemical Name: (CH₃)3CC₆H₄C(NC₆H₃(CH(CH₃)2)2)2^(1-)*Pb⁽²⁺⁾*O₃SCF₃^(1-)*OC₄H₈=((CH₃)3CC₆H₄C(NC₆H₃(CH(CH₃)2)2)2)Pb(O₃SCF₃)(OC₄H₈)
• CAS No.: 1301753-77-4
• Molecular Formula: CF₃O₃S*C₄H₈O*C₃₅H₄₇N₂*Pb
• Molecular Weight: 924.149

Synonyms:(CH₃)3CC₆H₄C(NC₆H₃(CH(CH₃)2)2)2^(1-)*Pb⁽²⁺⁾*O₃SCF₃^(1-)*OC₄H₈=((CH₃)3CC₆H₄C(NC₆H₃(CH(CH₃)2)2)2)Pb(O₃SCF₃)(OC₄H₈)

Chemical Property of (CH₃)3CC₆H₄C(NC₆H₃(CH(CH₃)2)2)2^(1-)*Pb⁽²⁺⁾*O₃SCF₃^(1-)*OC₄H₈=((CH₃)3CC₆H₄C(NC₆H₃(CH(CH₃)2)2)2)Pb(O₃SCF₃)(OC₄H₈)

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Technology Process of (CH₃)3CC₆H₄C(NC₆H₃(CH(CH₃)2)2)2^(1-)*Pb⁽²⁺⁾*O₃SCF₃^(1-)*OC₄H₈=((CH₃)3CC₆H₄C(NC₆H₃(CH(CH₃)2)2)2)Pb(O₃SCF₃)(OC₄H₈)

There total 1 articles about (CH₃)3CC₆H₄C(NC₆H₃(CH(CH₃)2)2)2^(1-)*Pb⁽²⁺⁾*O₃SCF₃^(1-)*OC₄H₈=((CH₃)3CC₆H₄C(NC₆H₃(CH(CH₃)2)2)2)Pb(O₃SCF₃)(OC₄H₈) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

(CH3)3CC6H4C(NC6H3(CH(CH3)2)2)2(1-)*K(1+)=((CH3)3CC6H4C(NC6H3(CH(CH3)2)2)2)K + lead(II) triflate (27607-92-7,56328-89-3,135179-19-0) → (CH3)3CC6H4C(NC6H3(CH(CH3)2)2)2(1-)*Pb(2+)*O3SCF3(1-)*OC4H8=((CH3)3CC6H4C(NC6H3(CH(CH3)2)2)2)Pb(O3SCF3)(OC4H8) (1301753-77-4)

Guidance literature:

In tetrahydrofuran; byproducts: KO3SCF3; under N2; soln. of K compd. in THF added to soln. of Pb compd. in THF at-78°C; warmed slowly to room temp.; stirred overnight; volatiles removed in vac.; extd. into pentane; concd.; crystd. at -30°C overnight;

DOI:10.1021/ic200682p

Reference yield:

(CH3)3CC6H4C(NC6H3(CH(CH3)2)2)2(1-)*Pb(2+)*O3SCF3(1-)*OC4H8=((CH3)3CC6H4C(NC6H3(CH(CH3)2)2)2)Pb(O3SCF3)(OC4H8) (1301753-77-4) → lead (7439-92-1) + (((CH3)3CC6H4C(NC6H3(CH(CH3)2)2)2)Pb)2 (1301753-85-4)

Guidance literature:

With (((Me₃C₆H₂NCMe)2CH)Mg)2; In not given; byproducts: 4-t-BuC6H4C(NC6H3-2,6-i-Pr2)2H; Pb complex treated with Mg compd.;

DOI:10.1021/ic200682p

upstream raw materials:

lead(II) triflate

Downstream raw materials:

lead

(((CH₃)3CC₆H₄C(NC₆H₃(CH(CH₃)2)2)2)Pb)2

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