C₉H₁₂ClF₃N₂OSi

Base Information

Chemical Name:C₉H₁₂ClF₃N₂OSi
CAS No.:1221172-07-1
Molecular Formula:C₉H₁₂ClF₃N₂OSi
Molecular Weight:284.741
Hs Code.:

C<sub>9</sub>H<sub>12</sub>ClF<sub>3</sub>N<sub>2</sub>OSi

Synonyms:C₉H₁₂ClF₃N₂OSi

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Chemical Property of C₉H₁₂ClF₃N₂OSi

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Technology Process of C₉H₁₂ClF₃N₂OSi

There total 1 articles about C₉H₁₂ClF₃N₂OSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1221171-70-5
2-chloro-6-(trifluoromethoxy)pyridine

: 1221172-07-1
C₉H₁₂ClF₃N₂OSi

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium; N-ethyl-N,N-diisopropylamine / tetrahydrofuran; hexane / 2 h / -78 °C

1.2: 1 h / 20 °C

2.1: n-butyllithium; 2,2,6,6-tetramethyl-piperidine / tetrahydrofuran; hexane / 3 h / -78 °C

2.2: 1 h / -78 °C

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 16 h / 0 - 20 °C

With 2,2,6,6-tetramethyl-piperidine; lithium aluminium tetrahydride; n-butyllithium; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; hexane;

Reference yield:

: 1221172-07-1
C₉H₁₂ClF₃N₂OSi

: 135900-33-3
3-amino-6-(trifluoromethoxy)pyridine

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 16 h / 25 °C

2: palladium 10% on activated carbon; ammonium formate / methanol / 16 h / 55 °C

With palladium 10% on activated carbon; tetrabutyl ammonium fluoride; ammonium formate; In tetrahydrofuran; methanol;

Reference yield:

: 1221172-07-1
C₉H₁₂ClF₃N₂OSi

: 1221172-05-9
3-amino-2-chloro-6-(trifluoromethoxy)pyridine

Guidance literature:: C₉H₁₂ClF₃N₂OSi; With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 25 ℃; for 20h;

With water; sodium hydroxide; In tetrahydrofuran;