2-(1-(5-methyl-1-(p-tolyl)-1H-1,2,3-triazol-4-yl)ethylidene)hydrazinecarbothioamide

Base Information

• Chemical Name: 2-(1-(5-methyl-1-(p-tolyl)-1H-1,2,3-triazol-4-yl)ethylidene)hydrazinecarbothioamide
• CAS No.: 1516632-10-2
• Molecular Formula: C₁₃H₁₆N₆S
• Molecular Weight: 288.376

Synonyms:2-(1-(5-methyl-1-(p-tolyl)-1H-1,2,3-triazol-4-yl)ethylidene)hydrazinecarbothioamide

Chemical Property of 2-(1-(5-methyl-1-(p-tolyl)-1H-1,2,3-triazol-4-yl)ethylidene)hydrazinecarbothioamide

Chemical Property:

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Technology Process of 2-(1-(5-methyl-1-(p-tolyl)-1H-1,2,3-triazol-4-yl)ethylidene)hydrazinecarbothioamide

There total 3 articles about 2-(1-(5-methyl-1-(p-tolyl)-1H-1,2,3-triazol-4-yl)ethylidene)hydrazinecarbothioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

thiosemicarbazide (79-19-6) + 1-[5-methyl-1-(p-tolyl)-1H-1,2,3-triazol-4-yl]ethanone → 2-(1-(5-methyl-1-(p-tolyl)-1H-1,2,3-triazol-4-yl)ethylidene)hydrazinecarbothioamide (1516632-10-2)

Guidance literature:

With acetic acid; In ethanol; for 3h; Reflux;

DOI:10.2174/157017861010131126115715

Reference yield:

p-methylazidobenzene (2101-86-2) → 2-(1-(5-methyl-1-(p-tolyl)-1H-1,2,3-triazol-4-yl)ethylidene)hydrazinecarbothioamide (1516632-10-2)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium ethanolate / 1 h / 0 °C

2: acetic acid / ethanol / 3 h / Reflux

With sodium ethanolate; acetic acid; In ethanol;

DOI:10.2174/157017861010131126115715

Reference yield:

acetylacetone (123-54-6,81235-32-7) → 2-(1-(5-methyl-1-(p-tolyl)-1H-1,2,3-triazol-4-yl)ethylidene)hydrazinecarbothioamide (1516632-10-2)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium ethanolate / 1 h / 0 °C

2: acetic acid / ethanol / 3 h / Reflux

With sodium ethanolate; acetic acid; In ethanol;

DOI:10.2174/157017861010131126115715

upstream raw materials:

p-methylazidobenzene

thiosemicarbazide

acetylacetone

Downstream raw materials:

2-(2-(1-(5-methyl-1-(p-tolyl)-1H-1,2,3-triazol-4-yl)ethylidene)hydrazinyl)-4-phenylthiazole

1-(1-(5-methyl-1-p-tolyl-1,2,3-triazol-4-yl)ethylidene)-2-(4-p-tolylthiazol-2-yl)hydrazine

1-(4-(4-methoxyphenyl)thiazol-2-yl)-2-(1-(5-methyl-1-p-tolyl-1,2,3-triazol-4-yl)ethylidene)hydrazine

1-(4-(4-chlorophenyl)thiazol-2-yl)-2-(1-(5-methyl-1-p-tolyl-1,2,3-triazol-4-yl)ethylidene)hydrazine

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