methyl 4,6-di-O-benzyl-3-C-methyl-2,3-di-O-(trimethylsilyl)-α-D-allopyranoside

Base Information

Chemical Name:methyl 4,6-di-O-benzyl-3-C-methyl-2,3-di-O-(trimethylsilyl)-α-D-allopyranoside
CAS No.:88567-48-0
Molecular Formula:C₂₈H₄₄O₆Si₂
Molecular Weight:532.825
Hs Code.:

Synonyms:methyl 4,6-di-O-benzyl-3-C-methyl-2,3-di-O-(trimethylsilyl)-α-D-allopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 4,6-di-O-benzyl-3-C-methyl-2,3-di-O-(trimethylsilyl)-α-D-allopyranoside

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Technology Process of methyl 4,6-di-O-benzyl-3-C-methyl-2,3-di-O-(trimethylsilyl)-α-D-allopyranoside

There total 4 articles about methyl 4,6-di-O-benzyl-3-C-methyl-2,3-di-O-(trimethylsilyl)-α-D-allopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.9%

: 75-77-4
chloro-trimethyl-silane

: 88567-47-9
methyl 4,6-di-O-benzyl-3-C-methyl-α-D-allopyranoside

: 88567-48-0
methyl 4,6-di-O-benzyl-3-C-methyl-2,3-di-O-(trimethylsilyl)-α-D-allopyranoside

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; Ambient temperature;
DOI:10.1016/0008-6215(83)84015-4

Reference yield:

: 58341-71-2
Methyl 4,6-di-O-benzyl-α-D-glucopyranoside

: 88567-48-0
methyl 4,6-di-O-benzyl-3-C-methyl-2,3-di-O-(trimethylsilyl)-α-D-allopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 97.8 percent / pyridine / Ambient temperature

2: 84.5 percent / pyridinium chlorochromate / CH₂Cl₂ / 24 h / Ambient temperature

3: 91.8 percent / diethyl ether; benzene / 5 h / Ambient temperature

4: 90.9 percent / imidazole / dimethylformamide / Ambient temperature

With 1H-imidazole; pyridinium chlorochromate; In pyridine; diethyl ether; dichloromethane; N,N-dimethyl-formamide; benzene;
DOI:10.1016/0008-6215(83)84015-4

Reference yield:

: 88567-45-7
methyl 2-O-benzoyl-4,6-di-O-benzyl-α-D-glucopyranoside

: 88567-48-0
methyl 4,6-di-O-benzyl-3-C-methyl-2,3-di-O-(trimethylsilyl)-α-D-allopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 84.5 percent / pyridinium chlorochromate / CH₂Cl₂ / 24 h / Ambient temperature

2: 91.8 percent / diethyl ether; benzene / 5 h / Ambient temperature

3: 90.9 percent / imidazole / dimethylformamide / Ambient temperature

With 1H-imidazole; pyridinium chlorochromate; In diethyl ether; dichloromethane; N,N-dimethyl-formamide; benzene;
DOI:10.1016/0008-6215(83)84015-4