(R)-ethyl 2-(4-(1-((tert-butoxycarbonyl)amino)-2-hydroxyethyl)phenoxy) acetate

Base Information

Chemical Name:(R)-ethyl 2-(4-(1-((tert-butoxycarbonyl)amino)-2-hydroxyethyl)phenoxy) acetate
CAS No.:1454273-76-7
Molecular Formula:C₁₇H₂₅NO₆
Molecular Weight:339.389
Hs Code.:

Synonyms:(R)-ethyl 2-(4-(1-((tert-butoxycarbonyl)amino)-2-hydroxyethyl)phenoxy) acetate

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Chemical Property of (R)-ethyl 2-(4-(1-((tert-butoxycarbonyl)amino)-2-hydroxyethyl)phenoxy) acetate

Chemical Property:

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Technology Process of (R)-ethyl 2-(4-(1-((tert-butoxycarbonyl)amino)-2-hydroxyethyl)phenoxy) acetate

There total 4 articles about (R)-ethyl 2-(4-(1-((tert-butoxycarbonyl)amino)-2-hydroxyethyl)phenoxy) acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 105-36-2
ethyl bromoacetate

: 691889-35-7
(R)-N-(t-butoxycarbonyl)-4-(t-butyldimethylsiloxy)phenylglycinol

: 1454273-76-7
(R)-ethyl 2-(4-(1-((tert-butoxycarbonyl)amino)-2-hydroxyethyl)phenoxy) acetate

Guidance literature:: With potassium carbonate; In acetone; at 20 - 80 ℃; for 15h;

Reference yield:

: 143323-49-3,141518-55-0
(R)-methyl 2-((tert-butoxycarbonyl)amino)-2-(4-hydroxyphenyl)acetate

: 1454273-76-7
(R)-ethyl 2-(4-(1-((tert-butoxycarbonyl)amino)-2-hydroxyethyl)phenoxy) acetate

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 20 °C

2: potassium carbonate / acetone / 15 h / 20 - 80 °C

With lithium aluminium tetrahydride; potassium carbonate; In tetrahydrofuran; acetone;

Reference yield:

: 22818-40-2
D-4-hydroxyphenylglycine

: 1454273-76-7
(R)-ethyl 2-(4-(1-((tert-butoxycarbonyl)amino)-2-hydroxyethyl)phenoxy) acetate

Guidance literature:: Multi-step reaction with 4 steps

1: thionyl chloride / Inert atmosphere; Cooling with ice; Reflux

2: triethylamine; sodium hydrogencarbonate / methanol; dichloromethane / 20 °C

3: lithium aluminium tetrahydride / tetrahydrofuran / 20 °C

4: potassium carbonate / acetone / 15 h / 20 - 80 °C

With lithium aluminium tetrahydride; thionyl chloride; sodium hydrogencarbonate; potassium carbonate; triethylamine; In tetrahydrofuran; methanol; dichloromethane; acetone;