N-<3-(2,3-dibenzyloxybenzoylamino)propyl>-N-<4-(2,3-dibenzyl-oxybenzoylamino)-butyl>-2,3-dibenzyloxybenzoyl-L-alanylamide

Base Information

Chemical Name:N-<3-(2,3-dibenzyloxybenzoylamino)propyl>-N-<4-(2,3-dibenzyl-oxybenzoylamino)-butyl>-2,3-dibenzyloxybenzoyl-L-alanylamide
CAS No.:161219-99-4
Molecular Formula:C₇₃H₇₂N₄O₁₀
Molecular Weight:1165.4
Hs Code.:

Synonyms:N-<3-(2,3-dibenzyloxybenzoylamino)propyl>-N-<4-(2,3-dibenzyl-oxybenzoylamino)-butyl>-2,3-dibenzyloxybenzoyl-L-alanylamide

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Chemical Property of N-<3-(2,3-dibenzyloxybenzoylamino)propyl>-N-<4-(2,3-dibenzyl-oxybenzoylamino)-butyl>-2,3-dibenzyloxybenzoyl-L-alanylamide

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Technology Process of N-<3-(2,3-dibenzyloxybenzoylamino)propyl>-N-<4-(2,3-dibenzyl-oxybenzoylamino)-butyl>-2,3-dibenzyloxybenzoyl-L-alanylamide

There total 3 articles about N-<3-(2,3-dibenzyloxybenzoylamino)propyl>-N-<4-(2,3-dibenzyl-oxybenzoylamino)-butyl>-2,3-dibenzyloxybenzoyl-L-alanylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 74272-81-4
2,3-bis(benzyloxy)-N-(3-(4-(2,3-bis(benzyloxy)benzamido)butylamino)propyl)benzamide

: 123198-04-9
N-<2,3-bis(benzyloxy)benzoyl>-L-alanine

: 161219-99-4
N-<3-(2,3-dibenzyloxybenzoylamino)propyl>-N-<4-(2,3-dibenzyl-oxybenzoylamino)-butyl>-2,3-dibenzyloxybenzoyl-L-alanylamide

Guidance literature:: With dmap; diphenylphosphoranyl azide; triethylamine; In N,N-dimethyl-formamide; 1.) 0 deg C; 2.) rt., 2 d;
DOI:10.1016/S0040-4020(01)85669-6

Reference yield:

: 69146-58-3
2,3-bis(benzyloxy)benzoyl chloride

: 161219-99-4
N-<3-(2,3-dibenzyloxybenzoylamino)propyl>-N-<4-(2,3-dibenzyl-oxybenzoylamino)-butyl>-2,3-dibenzyloxybenzoyl-L-alanylamide

Guidance literature:: Multi-step reaction with 3 steps

2: aq. sodium hydroxide

3: 72 percent / 1.) diphenylphosphoryl azide; 2.) triethylamine, dimethylaminopyridine / dimethylformamide / 1.) 0 deg C; 2.) rt., 2 d

With dmap; sodium hydroxide; diphenylphosphoranyl azide; triethylamine; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)85669-6

Reference yield:

: (S)-2-(2,3-Bis-benzyloxy-benzoylamino)-propionic acid methyl ester

: 161219-99-4
N-<3-(2,3-dibenzyloxybenzoylamino)propyl>-N-<4-(2,3-dibenzyl-oxybenzoylamino)-butyl>-2,3-dibenzyloxybenzoyl-L-alanylamide

Guidance literature:: Multi-step reaction with 2 steps

1: aq. sodium hydroxide

2: 72 percent / 1.) diphenylphosphoryl azide; 2.) triethylamine, dimethylaminopyridine / dimethylformamide / 1.) 0 deg C; 2.) rt., 2 d

With dmap; sodium hydroxide; diphenylphosphoranyl azide; triethylamine; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)85669-6