3-[3-(4,4-Dimethyl-4,5-dihydro-oxazol-2-yl)-2-methoxy-phenyl]-propan-1-ol

Base Information

Chemical Name:3-[3-(4,4-Dimethyl-4,5-dihydro-oxazol-2-yl)-2-methoxy-phenyl]-propan-1-ol
CAS No.:75934-05-3
Molecular Formula:C₁₅H₂₁NO₃
Molecular Weight:263.337
Hs Code.:

Synonyms:3-[3-(4,4-Dimethyl-4,5-dihydro-oxazol-2-yl)-2-methoxy-phenyl]-propan-1-ol

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Chemical Property of 3-[3-(4,4-Dimethyl-4,5-dihydro-oxazol-2-yl)-2-methoxy-phenyl]-propan-1-ol

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Technology Process of 3-[3-(4,4-Dimethyl-4,5-dihydro-oxazol-2-yl)-2-methoxy-phenyl]-propan-1-ol

There total 6 articles about 3-[3-(4,4-Dimethyl-4,5-dihydro-oxazol-2-yl)-2-methoxy-phenyl]-propan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 119-36-8,8024-54-2
methyl salicylate

: 75934-05-3
3-[3-(4,4-Dimethyl-4,5-dihydro-oxazol-2-yl)-2-methoxy-phenyl]-propan-1-ol

Guidance literature:: Multi-step reaction with 5 steps

1: potassium carbonate / acetone / 60 h

2: sodium hydride / 1) 20 min at 0 deg C 2) reflux for 12 h

3: sodium hydroxide / 1) 1h reflux with NaOH 2) concentrated HCl

4: thionyl chloride

5: sodium hydroxide; boron trifluoride-tetrahydrofuran complex; dihydrogen peroxide / 2) at 55-60 deg C for 90 min

With sodium hydroxide; thionyl chloride; boron trifluoride-tetrahydrofuran complex; dihydrogen peroxide; sodium hydride; potassium carbonate; In acetone;
DOI:10.1021/jo00317a027

Reference yield:

: 75934-02-0
2-(3-allyl-2-methoxyphenyl)-4,4-dimethyl-4,5-dihydrooxazole

: 75934-05-3
3-[3-(4,4-Dimethyl-4,5-dihydro-oxazol-2-yl)-2-methoxy-phenyl]-propan-1-ol

Guidance literature:: With sodium hydroxide; boron trifluoride-tetrahydrofuran complex; dihydrogen peroxide; Yield given. Multistep reaction; 2) at 55-60 deg C for 90 min;
DOI:10.1021/jo00317a027

Reference yield:

: 75934-00-8
2-Allyl-6-(carbomethoxy)anisole

: 75934-05-3
3-[3-(4,4-Dimethyl-4,5-dihydro-oxazol-2-yl)-2-methoxy-phenyl]-propan-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide / 1) 1h reflux with NaOH 2) concentrated HCl

2: thionyl chloride

3: sodium hydroxide; boron trifluoride-tetrahydrofuran complex; dihydrogen peroxide / 2) at 55-60 deg C for 90 min

With sodium hydroxide; thionyl chloride; boron trifluoride-tetrahydrofuran complex; dihydrogen peroxide;
DOI:10.1021/jo00317a027