RhCN(tris(2-(diphenylphosphino)ethyl)phosphine)

Base Information

Chemical Name:RhCN(tris(2-(diphenylphosphino)ethyl)phosphine)
CAS No.:118681-54-2
Molecular Formula:C₄₃H₄₂NP₄Rh
Molecular Weight:799.614
Hs Code.:

Synonyms:RhCN(tris(2-(diphenylphosphino)ethyl)phosphine)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of RhCN(tris(2-(diphenylphosphino)ethyl)phosphine)

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Technology Process of RhCN(tris(2-(diphenylphosphino)ethyl)phosphine)

There total 3 articles about RhCN(tris(2-(diphenylphosphino)ethyl)phosphine) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: potassium cyanide

: 109786-30-3
tris(2-diphenylphosphanylethyl)phosphanerhodium(I) hydride

: 333-27-7
methyl trifluoromethanesulfonate

: 118681-54-2
RhCN(tris(2-(diphenylphosphino)ethyl)phosphine)

Guidance literature:: In tetrahydrofuran; methanol; byproducts: CH4; CH3OH soln. of KCN added (N2) to soln. of complex in THF (treated with MeOSO2CF3); ethanol added, concd., collected on sintered glass frits, washed (EtOH, pentane), dried (N2); elem. anal.;

Reference yield: 75.0%

: 122874-55-9
Rh(acetone)(tris(2-(diphenylphosphino)ethyl)phosphine) tetrafluoroborate

: 118681-54-2
RhCN(tris(2-(diphenylphosphino)ethyl)phosphine)

Guidance literature:: With NaCN; In acetone; N2; excess of NaCN, addn. of 15-crown-5, soln. stirred for 30 min at room temp.; ppt. washed with EtOH/Et2O, dried in vac.;

Reference yield: 70.0%

: 109786-30-3
tris(2-diphenylphosphanylethyl)phosphanerhodium(I) hydride

: 623-49-4
ethyl cyanoformate

: 118681-54-2
RhCN(tris(2-(diphenylphosphino)ethyl)phosphine)

: 109-94-4
formic acid ethyl ester

Guidance literature:: In tetrahydrofuran; neat formate pipetted into soln. of complex, heated at ca. 40°C (20-30 min), cooled to room temp.; ethanol/n-hexane 1:1 added, concd. (N2), crystals collected on sintered glass frits, washed (EtOH, pentane), dried (N2);