3-phenyl-2,2-(bis(dicyclohexylamino)phosphino)(trimethylsilyl)-2H-aziridine

Base Information

• Chemical Name: 3-phenyl-2,2-(bis(dicyclohexylamino)phosphino)(trimethylsilyl)-2H-aziridine
• CAS No.: 167955-65-9
• Molecular Formula: C₃₅H₅₈N₃PSi
• Molecular Weight: 579.925

Synonyms:3-phenyl-2,2-(bis(dicyclohexylamino)phosphino)(trimethylsilyl)-2H-aziridine

Chemical Property of 3-phenyl-2,2-(bis(dicyclohexylamino)phosphino)(trimethylsilyl)-2H-aziridine

Chemical Property:

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Technology Process of 3-phenyl-2,2-(bis(dicyclohexylamino)phosphino)(trimethylsilyl)-2H-aziridine

There total 2 articles about 3-phenyl-2,2-(bis(dicyclohexylamino)phosphino)(trimethylsilyl)-2H-aziridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

benzonitrile (100-47-0) + [bis(dicyclohexylamino)phosphino](trimethylsilyl)carbene (152387-46-7,156280-08-9) → 3-phenyl-2,2-(bis(dicyclohexylamino)phosphino)(trimethylsilyl)-2H-aziridine (167955-65-9)

Guidance literature:

In toluene; Ambient temperature;

DOI:10.1080/10426509608545182

Reference yield: 78.0%

benzonitrile (100-47-0) + [Bis(dicyclohexylamino)phosphanyl](trimethylsilyl)diazomethane (145397-27-9) → 3-phenyl-2,2-(bis(dicyclohexylamino)phosphino)(trimethylsilyl)-2H-aziridine (167955-65-9)

Guidance literature:

In toluene; at 75 ℃; for 18h;

DOI:10.1002/chem.19970031106

Reference yield: 98.0%

3-phenyl-2,2-(bis(dicyclohexylamino)phosphino)(trimethylsilyl)-2H-aziridine (167955-65-9) → [2-Bis(dicyclohexylamino)-4-phenyl-2-trimethylsilyl]-2λ5-azaphosphete (167955-66-0)

Guidance literature:

In pentane; for 19h; Irradiation;

DOI:10.1002/chem.19970031106

upstream raw materials:

benzonitrile

[bis(dicyclohexylamino)phosphino](trimethylsilyl)carbene

[Bis(dicyclohexylamino)phosphanyl](trimethylsilyl)diazomethane

Downstream raw materials:

[2-Bis(dicyclohexylamino)-4-phenyl-2-trimethylsilyl]-2λ⁵-azaphosphete

C₃₇H₆₁N₄PSSi

2-[Bis(dicyclohexylamino)thioxophosphoranyl]-3-phenyl-2-trimethylsilyl-2H-azirine

2,2-Bis-dicyclohexylamino-1-methyl-4-phenyl-3-trimethylsilanyl-1H-2λ⁵-[1,5,2]diazaphosphinine-6-thione

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