2-[Bis(dicyclohexylamino)thioxophosphoranyl]-3-phenyl-2-trimethylsilyl-2H-azirine

Base Information

Chemical Name:2-[Bis(dicyclohexylamino)thioxophosphoranyl]-3-phenyl-2-trimethylsilyl-2H-azirine
CAS No.:200071-04-1
Molecular Formula:C₃₅H₅₈N₃PSSi
Molecular Weight:611.991
Hs Code.:

Synonyms:2-[Bis(dicyclohexylamino)thioxophosphoranyl]-3-phenyl-2-trimethylsilyl-2H-azirine

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Chemical Property of 2-[Bis(dicyclohexylamino)thioxophosphoranyl]-3-phenyl-2-trimethylsilyl-2H-azirine

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Technology Process of 2-[Bis(dicyclohexylamino)thioxophosphoranyl]-3-phenyl-2-trimethylsilyl-2H-azirine

There total 4 articles about 2-[Bis(dicyclohexylamino)thioxophosphoranyl]-3-phenyl-2-trimethylsilyl-2H-azirine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 167955-65-9
3-phenyl-2,2-(bis(dicyclohexylamino)phosphino)(trimethylsilyl)-2H-aziridine

: 200071-04-1
2-[Bis(dicyclohexylamino)thioxophosphoranyl]-3-phenyl-2-trimethylsilyl-2H-azirine

Guidance literature:: With sulfur; In tetrahydrofuran; for 1h; Ambient temperature;
DOI:10.1002/chem.19970031106

Reference yield:

: 100-47-0
benzonitrile

: 200071-04-1
2-[Bis(dicyclohexylamino)thioxophosphoranyl]-3-phenyl-2-trimethylsilyl-2H-azirine

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / toluene / 18 h / Ambient temperature

2: 91 percent / S₈ / tetrahydrofuran / 1 h / Ambient temperature

With sulfur; In tetrahydrofuran; toluene;
DOI:10.1002/chem.19970031106

Reference yield:

: 145397-27-9
[Bis(dicyclohexylamino)phosphanyl](trimethylsilyl)diazomethane

: 200071-04-1
2-[Bis(dicyclohexylamino)thioxophosphoranyl]-3-phenyl-2-trimethylsilyl-2H-azirine

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / toluene / 18 h / 75 °C

2: 91 percent / S₈ / tetrahydrofuran / 1 h / Ambient temperature

With sulfur; In tetrahydrofuran; toluene;
DOI:10.1002/chem.19970031106