C₂₁H₁₉⁽²⁾H₂NO₂

Base Information

Chemical Name:C₂₁H₁₉⁽²⁾H₂NO₂
CAS No.:1361110-38-4
Molecular Formula:C₂₁H₂₁NO₂
Molecular Weight:321.387
Hs Code.:

C<sub>21</sub>H<sub>19</sub><sup>(2)</sup>H<sub>2</sub>NO<sub>2</sub>

Synonyms:C₂₁H₁₉⁽²⁾H₂NO₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₁H₁₉⁽²⁾H₂NO₂

Chemical Property:

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Technology Process of C₂₁H₁₉⁽²⁾H₂NO₂

There total 6 articles about C₂₁H₁₉⁽²⁾H₂NO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67-56-1
methanol

: 1361111-14-9
C₂₀H₁₆⁽²⁾H₂N₂

: 1361110-38-4
C₂₁H₁₉⁽²⁾H₂NO₂

Guidance literature:: methanol; C₂₀H₁₆⁽²⁾H₂N₂; With sulfuric acid; at 0 ℃; Reflux;

With water; sodium hydrogencarbonate; In methanol;
DOI:10.1016/j.tetlet.2012.01.004

Reference yield:

: 1361110-35-1
methyl 3-(benzylamino)-2,2-dideutero-3-(4-bromophenyl)propanoate

: 1361110-38-4
C₂₁H₁₉⁽²⁾H₂NO₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: palladium on activated charcoal; ammonium formate

2.1: potassium carbonate / methanol / 20 °C

3.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

3.2: 4 h / -78 °C / Inert atmosphere

3.3: Saturated solution

4.1: sulfuric acid / 0 °C / Reflux

With sulfuric acid; palladium on activated charcoal; ammonium formate; potassium carbonate; lithium diisopropyl amide; In tetrahydrofuran; methanol;
DOI:10.1016/j.tetlet.2012.01.004

Reference yield:

: 1361111-11-6
C₁₆H₁₃⁽²⁾H₂BrN₂

: 1361110-38-4
C₂₁H₁₉⁽²⁾H₂NO₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: sulfuric acid / 0 °C / Reflux

2.1: palladium on activated charcoal; ammonium formate

3.1: potassium carbonate / methanol / 20 °C

4.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

4.2: 4 h / -78 °C / Inert atmosphere

4.3: Saturated solution

5.1: sulfuric acid / 0 °C / Reflux

With sulfuric acid; palladium on activated charcoal; ammonium formate; potassium carbonate; lithium diisopropyl amide; In tetrahydrofuran; methanol;
DOI:10.1016/j.tetlet.2012.01.004