2-Methyldibenzothiophene

Base Information

Chemical Name:2-Methyldibenzothiophene
CAS No.:20928-02-3
Molecular Formula:C13H10 S
Molecular Weight:198.288
Hs Code.:2934999090
European Community (EC) Number:621-740-6
DSSTox Substance ID:DTXSID90904785
Nikkaji Number:J467.071J
Wikidata:Q81988281
Mol file:20928-02-3.mol

Synonyms:2-METHYLDIBENZOTHIOPHENE;20928-02-3;2-Methyldibenzo[b,d]thiophene;Dibenzothiophene, 2-methyl-;2-methyl-dibenzothiophene;30995-64-3;Methyldibenzothiophene, 2-;2-methyl dibenzo[b]thiophene;SCHEMBL257003;Dibenzo[b]thiophene, 2-methyl;DTXSID90904785;AKOS006275434;FT-0692546

Suppliers and Price of 2-Methyldibenzothiophene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2-Methyldibenzothiophene
10mg
$ 105.00

Medical Isotopes, Inc.
2-Methyldibenzothiophene
250 mg
$ 2200.00

American Custom Chemicals Corporation
2-METHYLDIBENZOTHIOPHENE 98.00%
5MG
$ 500.72

Total 8 raw suppliers

Chemical Property of 2-Methyldibenzothiophene

Chemical Property:

Melting Point:85.5 °C
Boiling Point:163-165 °C(Press: 3 Torr)
PSA：28.24000
Density:1.213±0.06 g/cm3(Predicted)
LogP:4.36290
Storage Temp.:Refrigerator, under inert atmosphere
Solubility.:Chloroform (Sparingly), Ethyl Acetate (Slightly)
XLogP3:4.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:198.05032149
Heavy Atom Count:14
Complexity:213

Purity/Quality:

98%Min ^*data from raw suppliers

2-Methyldibenzothiophene ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC2=C(C=C1)SC3=CC=CC=C32
Uses 2-Methyldibenzothiophene, is an alkyldibenzothiophene present in crude oil. Research concerning the biodegradation of Dibenzothiophene by different types of bacteria is a currently being carried out, as these bacteria have the ability to breakdown other harmful PAH’s as well. This may be used in removing spilled oil from marine and terrestrial environments.

Technology Process of 2-Methyldibenzothiophene

There total 3 articles about 2-Methyldibenzothiophene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 1205612-12-9
2,5-di-p-tolyl-N[2-(allylthio)phenyl]pyrrole

: 20928-02-3
2-methyldibenzothiophene

: 1205611-78-4
1-p-tolylpyrrolo[2,1-b]benzothiazole

: 1205611-80-8
6-methyl-1-p-tolyldibenzo[b,f]pyrrolo[1,2-d]-1,4-thiazepine

: 1205611-85-3
10-methyl-2-p-tolyl-1H-dibenzo[2,3:6,7]thiepino[4,5-b]pyrrole

: 1205611-82-0
4-methyl-1-(5-p-tolylpyrrol-2-yl)dibenzothiophene

Guidance literature:: at 650 ℃; for 0.25h; under 0.005 Torr; Pyrolysis; Gas phase;
DOI:10.1039/b914965a

Reference yield: 34.0%

: 930-69-8
sodium thiophenolate

: 2-chloro-4-methylbenzenediazonium tetrafluoroborate

: 20928-02-3
2-methyldibenzothiophene

: 107701-44-0
3-chloro-1-methyl-4-(phenylsulfonyl)benzene

: 107701-45-1
1,2-bis(phenylsulfonyl)-4-methylbenzene

Guidance literature:: With dihydrogen peroxide; Yield given. Multistep reaction; 1.) DMSO, 25 degC, 320 min, 2.) glacial acetic acid, 100 degC;
DOI:10.1016/S0040-4020(01)87556-6

Reference yield:

: 6320-03-2
2-chlorothiphenol

: C₁₃H₁₀ClIO₃S

: 16587-52-3
3-methyl-dibenzothiophene

: 20928-02-3
2-methyldibenzothiophene

Guidance literature:: 2-chlorothiphenol; C₁₃H₁₀ClIO₃S; With isopropylmagnesium chloride; In tetrahydrofuran; at -78 ℃; for 0.75h; Inert atmosphere; Sealed tube; Cooling with acetone-dry ice;

With (1,2-dimethoxyethane)dichloronickel(II); triphenylphosphine; In tetrahydrofuran; at 0 - 30 ℃; for 16h; Reagent/catalyst; Inert atmosphere; Cooling with ice;
DOI:10.1021/acs.orglett.5b01115